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GCMS calibration results for volatile organics, February 2002

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Calibration report for GCMS analysis of volatile organic compounds including nitrosamines and chlorinated solvents from February 2002.

NYC-WTC_000052676–000052679

Folder label: “GCMS X 1/15/02 A 2/11/02

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NYC 9/11 Public Portal Document

wC/

Data File C: \HPCHEM\ 1 \DATA\ FEB110 2 \CAL8 0 . D Vial: 2 Acq On 11 Feb 2002 11:12 am Operator: 209 GALOS ) Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 19 9:41 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.38 168 1711769 84.21 ug/1 # 91 31) 4-Bromophenyl-phenylether 24.43 248 1105688 84.16 ug/1 98 32) Hexachlorobenzene 24.88 284 1278316 83.08 ug/1 97 33) Phenanthrene 25.86 178 5433032 86.65 ug/1 100 34) Anthracene 26.00 178 5385964 87.68 ug/1 100 35) Di-n-butylphthalate 27.74 149 7580412 86.51 ug/1 99 36) Fluoranthene 29.49 202 5587983 89.28 ug/1 # 92 3 9) Pyrene 30.18 202 5687835 80.99 ug/1 94 40) Butylbenzylphthalate 32.28 149 3138442 80.71 ug/1 99 41) Benzo(a)anthracene 33.81 228 4452741 86.71 ug/1 100 42) Bis(2-ethylhexyl)phthalate 34.05 149 4063312 77.35 ug/1 98 43) Chrysene 33.95 228 4350647 86.10 ug/1 99 45) Di-n-Octylphthalate 35.80 149 6230256 78.09 ug/1 # 99 46) Benzo(b)fluoranthene 36.95 252 4138578 91.92 ug/1 99 47) Benzo(k)fluoranthene 37.04 252 3988645 88.15 ug/1 98 48) Benzo(a)pyrene 37.98 252 3344977 89.63 ug/1 98 49) Indeno(1,2,3-cd)pyrene 42.44 276 3209461 94.23 ug/1 97 50) Dibenz(a,h)anthracene 42.52 278 2546894 97.84 ug/1 98 51) Benzo(g,h,i)perylene 43.75 276 2447504m 89.14 ug/1

(#) = qualifier out of range (m) = manual integration CAL80.D GCMS0208.M Tue Feb 19 09:41:38 2002 Page 2

NYC-WTC_000052678

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NYC-WTC_000052678Source: NYC Law Department, mirrored locally

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