GCMS analysis results for sample AE03833, Mar 13 2002

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Data File C:\HPCHEM\1\DATA\FEB2102\CAL4 OC.D Vial: 2 Acq On 24 Feb 2002 1:56 pm Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 13 16:01 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 12.34 152 410532 20.00 ug/1 -0.01 10) Naphthalene-d8 15.99 136 1636801 20.00 ug/1 0.00 17) Acenaphthene-diO 21.30 164 883397 20.00 ug/1 -0.01 29) Phenanthrene-diO 25.75 188 1386873 20.00 ug/1 -0.01 38) Chrysene-dl2 33.83 240 923622 20.00 ug/1 -0.01 44) Perylene-dl2 38.11 264 579814 20.00 ug/1 -0.01

System Monitoring Compounds 37) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.97 74 791784 48.20 ug/1 # 77 3) bis(2-Chloroethyl)ether 11.76 93 1186164 43.96 ug/1 94 4) 1,3-Dichlorobenzene 12.25 146 1197096 37.27 ug/1 100 5) 1,4-Dichiorobenzene 12.39 146 1203897 36.78 ug/1 100 6) 1,2-Diehlorobenzene 12.91- 146 1107620 35.61 ug/1 100 7) 2,2'-oxybis(1-Chloropropan 13.22 45 1711309 41.89 ug/1 98 8) N-Nitroso-di-n-propylamine 13.64 70 849155 43.99 ug/1 88 9) Hexachloroethane 13.75 117 467339 35.67 ug/1 96 11) Nitrobenzene 14.05 77 1208991 35.92 ug/1 96 12) Isophorone 14.70 82 2353446 41.39 ug/1 98 13) bis(2-Chloroethoxy)methane 15.37 93 1442907 40.75 ug/1 98 14) 1,2,4-Trichlorobenzene 15.87 180 978353 34.93 ug/1 98 15) Naphthalene 16.05 128 3116356 35.75 ug/1 99 16) Hexachlorobutadiene 16.58 225 499604 (29.80 ug/l 100 18) Hexachlorocyclopentadiene 18.77 237 375922 29.72 ug/1 99 19) 2-Chloronaphthalene 19.56 162 1938643 36.81 ug/1 99 20) Dimethylphthalate 20.66 163 2329307 37.98 ug/1 99 21) 2,6-Dinitrotoluene 20.88 165 567455 40.82 ug/1 90 22) Acenaphthylene 20.83 152 2893907 38.03 ug/1 99 23) Ac enapht hene 21.41 153 1959364 36.84 ug/1 98 24) 2,4-Dinitrotoluene 22.05 165 766111 43.50 ug/1 87 25) Diethylphthalate 22.80 149 2334423 36.62 ug/1 97 26) 4-Chlorophenyl-phenylether 22.94 204 900699 32.82 ug/1 98 27) Fluorene 22.92 166 1987289 34.24 ug/1 100 28) Azobenzen/ 1,2-Diphenylhyd 23.42 77 2529805m 37.73 ug/L

(#) = qualifier out of range (m) = manual integration CAL40C.D GCMS0208.M Wed Mar 13 16:01:36 2002 Page 1

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