GCMS analysis results for sample AE04028, March 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\MAR22O2\REFB1.D Vial: 33 Acq On : 24 Mar 2002 1:40 am Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 26 8:32 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.26 152 479275 • 20.00 ug/1 -0.09 10) Naphthalene-d8 15.91 136 1907227 20.00 ug/1 -0.09 17) Acenaphthene-dlO 21.21 164 1089885 20.00 ug/1 -0.10 29) Phenanthrene-diO 25.66 188 1666493 20.00 ug/1 -0.11 38) Chrysene-dl2 33.73 240 1098270 20.00 ug/1 -0.12 44) Perylene-dl2 37.98 264 647009 20.00 ug/1 -0.14

System Monitoring Compounds 37) 2,4-DDD 30.73 235 84122 6.95 ug/mL 0.24 Spiked Amount 5.000 Recovery = 139.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.90 74 79496 4.89 ug/1 # 69 3) bis(2-Chloroethyl)ether 11.66 93 196184 7.49 ug/1 93 4) 1,3-Dichlorobenzene 12.16 146 78925 2.92 ug/1 98 5) 1,4-Dichlorobenzene 12.31 146 88468 3.26 ug/1 99 6) 1,2-Dichlorobenzene 12.82- 146 100996 3.99 ug/1 98 7) 2,21-oxybis(1-Chloropropan 13.15 45 273115 7.41 ug/1 99 8) N-Nitroso-di-n-propylamine 13.53 70 137636 8.08 ug/1 # 86 9) Hexachloroethane 13.68 117 15962 1.57 ug/1 # 88 11) Nitrobenzene 13.94 77 180015 6.90 ug/1 91 12) Isophorone 14.60 82 410586 8.30 ug/1 98 13) bis(2-Chloroethoxy)methane 15.27 93 247686 7.65 ug/1 98 14) 1,2,4-Trichlorobenzene 15.79 180 93370 4.17 ug/1 98 15) Naphthalene 15.96 128 471225 6.68 ug/1 99 16) Hexachlorobutadiene 16.51 225 14329 1.28 ug/1 96 18) Hexachlorocyclopentadiene 18.70 237 6518 0.88 ug/1 # 86 19) 2-Chloronaphthalene 19.47 162 296892 6.34 ug/1 96 20) Dimethylphthalate 20.55 163 457545 8.34 ug/1 98 21) 2,6-Dinitrotoluene 20.77 165 97924 7.36 ug/1 # 78 22) Acenaphthylene 20.74 152 521041 7.79 ug/1 99 23) Acenaphthene 21.31 153 351778 7.52 ug/1 98 24) 2,4-Dinitrotoluene 21.94 165 123076 6.91 ug/1 # 78 25) Diethylphthalate 22.69 149 447920 8.41 ug/1 # 94 26) 4-Chlorophenyl-phenylether 22.85 204 184463 8.09 ug/1 90 27) Fluorene 22.82 166 402631 8.14 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.31 77 383007 6.71 ug/L # 85

(#) = qualifier out of range (m) = manual integration REFB1.D GCMS0308.M Tue Mar 26 08:35:33 2002 Page 1

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