GCMS reference standard report, May 6, 2002

NYC 9/11 Public Portal Document

Data File C:\HPCHEM\l\DATA\MAY0602\REF2.D Vial: 5 Acq On 6 May 2002 1:25 pm Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 8 9:35 2002 Quant Results File: GCMS0501.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.19 152 508220 40.00 ug/1 -0.02 10) Naphthalene-d8 15.83 136 1861319 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.14 164 1017640 40.00 ug/1 -0.01 30) Phenanthrene-diO 25.57 188 1445132 40.00 ug/1 -0.02 38) Chrysene-dl2 33.64 240 988646 40.00 ug/1 -0.03 44) Perylene-dl2 37.86 264 661061 40.00 ug/1 -0.02

System Monitoring Compounds 28) TCMX 23.27 209 32484 6.56 ug/L -0.02 Spiked Amount 10.000 Recovery = 65.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.83 74 97555 7.02 ug/1 99 3) bis(2-Chloroethyl)ether 11.59 93 188934 10.48 ug/1 97 4) 1,3-Dichlorobenzene 12.09 146 135219 8.54 ug/1 98 5) 1,4-Dichlorobenzene 12.24 146 145285 8.39 ug/1 99 6) 1,2-Dichlorobenzene 12.75 146 144584 9.63 ug/1 98 7) 2,2'-oxybis(1-Chloropropan 13.07 45 395028 10.60 ug/1 99 8) N-Nitroso-di-n-propylamine 13.46 70 138111 10.22 ug/1 97 9) Hexachloroethane 13.60 117 36436 5.60 ug/1 93 11) Nitrobenzene 13.87 77 171020 10.09 ug/1 99 12) Isophorone 14.52 82 398062 12.11 ug/1 97 13) bis(2-Chloroethoxy)methane 15.20 93 226153 10.84 ug/1 99 14) 1,2,4-Trichlorobenzene 15.71 180 120087 9.53 ug/1 100 15) Naphthalene 15.89 128 459830 11.80 ug/1 100 16) Hexachlorobutadiene 16.43 225 38884 6.71 ug/1 99 18) Hexachlorocyclopentadiene 18.63 237 16765 3.25 ug/1 96 19) 2-Chloronaphthalene 19.39 162 275419 12.26 ug/1 99 20) Dimethylphthalate 20.48 163 337742 11.81 ug/1 100 21) 2,6-Dinitrotoluene 20.70 165 61839 9.95 ug/1 95 22) Acenaphthylene 20.66 152 440591 10.90 ug/1 99 23) Acenaphthene 21.22 153 291441 12.28 ug/1 99 24) 2,4-Dinitrotoluene 21.86 165 70133 10.52 ug/1 96 25) Diethylphthalate 22.61 149 335245 12.92 ug/1 99 26) 4-Chlorophenyl-phenylether 22.77 204 144874 11.80 ug/1 99 27) Fluorene 22.74 166 321068 12.70 ug/1 98 29) Azobenzen/ 1,2-Diphenylhyd 23.23 77 360672 10.35 ug/L 99 31) N-Nitrosodiphenylamine 23.15 168 115923 12.10 ug/1 96 32) 4-Bromophenyl-phenylether 24.23 248 79910 11.38 ug/1 99 33) Hexachlorobenzene 24.67 284 98640 12.58 ug/1 96 34) Phenanthrene 25.64 178 429091 12.25 ug/1 99

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0501.M Wed May 08 09:36:39 2002 Page 1

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