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GCMS analysis results for sample AE04028, March 2002

Machine-extracted title · confidence 95%

Laboratory report listing gas chromatography-mass spectrometry detection of volatile organic compounds in environmental sample AE04028.

NYC-WTC_000038494–000038501

Folder label: “GCMS X 2/25/02 A 3/23/02

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Scanned page image, NYC-WTC_000038497
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NYC 9/11 Public Portal Document (QT Reviewed) quantitation Report

Data File : C:\HPCHEM\1\DATA\MAR22O2\REFB1.D Vial: 33 Acq On : 24 Mar 2002 1:40 am Operator : Sample : gc/ms scan 2/25 Inst : GC/MS 2 09 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 26 8:32 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.23 168 162286 7.21 ug/1 # 81 31) 4-Bromophenyl-phenylether 24.32 248 101328 7.66 ug/1 # 90 32) Hexachlorobenzene 24.75 284 109035 7.10 ug/1 # 89 33) Phenanthrene 25.72 178 578730 8.04 ug/1 99 34) Anthracene 25.85 178 541615 7.59 ug/1 99 35) Di-n-butylphthalate 27.62 149 780944 8.62 ug/1 98 36) Fluoranthene 29.35 202 587816 7.78 ug/1 # 94 39) Pyrene 30.03 202 609987 9.67 ug/1 # 94 40) Butylbenzylphthalate 32.16 149 269089 8.28 ug/1 98 41) Benzo(a)anthracene 33.66 228 412965 7.87 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.93 149 373127 8.50 ug/1 95 43) Chrysene 33.79 228 425688 8.28 ug/1 99 45) Di-n-Octylphthalate 35.67 149 410036 7.19 ug/1 # 97 46) Benzo(b)fluoranthene 36.78 252 316361 8.01 ug/1 97 47) Benzo(k)fluoranthene 36.84 252 350048 9.09 ug/1 # 96 48) Benzo(a)pyrene 37.77 252 247927 6.89 ug/1 # 96 49) Indeno(1,2,3-cd)pyrene 42.11 276 244134 5.61 ug/1 98 50) Dibenz(a,h)anthracene 42.18 278 207611 6.17 ug/1 # 94 51) Benzo(g,h,i)perylene 43.35 276 205562 5.80 ug/1 96

(#) = qualifier out of range (m) = manual integration REFB1.D GCMS0308.M Tue Mar 26 08:35:36 2002 Page 2

NYC-WTC_000038497

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NYC-WTC_000038497Source: NYC Law Department, mirrored locally

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