GCMS analysis results for sample AE03833, Mar 13 2002

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Data File C:\HPCHEM\1\DATA\FEB210 2\CAL4 0C.D Vial: 2 Acq On 24 Feb 2002 1:56 pm Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 13 16:01 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.35 168 945500 34.77 ug/1 # 90 31) 4-Bromophenyl-phenylether 24.41 248 540808 30.77)ug/1 97 32) Hexachlorobenzene 24.85 284 616405 29.95 ug/1 97 3 3) Phenanthrene 25.83 178 2944122 35.10 ug/1 100 34) Anthracene 25.96 178 2842819 34.59 ug/1 99 35) Di-n-butylphthalate 27.72 149 3891170 33.20 ug/1 99 36) Fluoranthene 29.46 202 3018039 36.04 ug/1 # 90 39) Pyrene 30.14 202 3068443 37.93 ug/1 # 89 40) Butylbenzylphthalate 32.25 149 1622683 36.23 ug/1 94 41) Benzo(a)anthracene 33.78 228 2217601 37.50 ug/1 99 42) Bis(2-ethylhexyl)phthalate 34.02 149 1962133 32.43 ug/1 96 43) Chrysene 33.91 228 2139575 36.76 ug/1 100 45) Di-n-Octylphthalate 35.77 149 3009662 32.41 ug/1 # 99 46) Benzo(b)fluoranthene 36.91 252 1958410 37.37 ug/1 # 96 47) Benzo(k)fluoranthene 36.99 252 2011705 38.20 ug/1 # 96 4 8) Benzo(a)pyrene 37.92 252 1658426 38.18 ug/1 # 95 49) Indeno(l,2,3-cd)pyrene 42.36 276 1687861 42.58 ug/1 # 92 50) Dibenz(a,h)anthracene 42.42 278 1293420 42.69 ug/1 # 94 51) Benzo(g,h,i)perylene 43.64 276 1358419 42.51 ug/1 # 94

(#) = qualifier out of range (m) = manual integration CAL40C.D GCMS0208.M Wed Mar 13 16:01:39 2002 Page 2

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