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GCMS analysis results, sample AE02785, March 2002

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analysis of sample AE02785 performed on 3/11/2002, detecting 2,4-DDD and other unknown compounds.

NYC-WTC_000005545–000005563

Folder label: “GCMS X 2/6/02 A 3/1/02

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NYC 9/11 Public Portal Document gUait- Lc L —L LCPUL

Data File C:\HPCHEM\l\DATA\MAR0102\2785.D Vial: 19 Acq On 2 Mar 2002 2:03 am Operator: Sample gc/ms scan 2/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 5 10:34 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 • N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.72 178 267 N.D. 3 4) Anthracene 25.72 178 267 N.D. 35) Di-n-butylphthalate 27.68 149 19328 N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.78 228 1704 N.D. 42) Bis(2-ethylhexyl)phthalate 33.99 149 3588 N.D. 43) Chrysene 33.78 228 1704 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 4 8) Benzo(a)pyrene 38.06 252 1834 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 2785.D GCMS0208.M Tue Mar 05 10:37:20 2002 Page 2

NYC-WTC_000005548

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NYC-WTC_000005548Source: NYC Law Department, mirrored locally

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