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GCMS analysis results for sample AE02567, March 2002

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Laboratory report listing quantitative results for volatile organic compounds in sample AE02567 analyzed on March 21, 2002.

NYC-WTC_000038752–000038755

Folder label: “GCMS X 3/4/02 A 3/20/02

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NYC 9/11 Public Portal Document LPW VV—/

Data File : C:\HPCHEM\1\DATA\MAR1902\CAL40.D Vial: 2 Acq On : 20 Mar 2002 9:55 am Operator: Sample : new Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 21 14:44 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.25 168 883641 36.70 ug/1 # 86 31) 4-Bromophenyl-phenylether 24.33 248 521705m 36.87 ug/1 32) Hexachlorobenzene 24.76 284 594268 36.17 ug/1 95 33) Phenanthrene 25.74 178 2859141 37.14 ug/1 99 34) Anthracene 25.87 178 2894887 37.92 ug/1 99 35) Di-n-butylphthalate 27.63 149 3575981 36.91 ug/1 99 36) Fluoranthene 29.37 202 2975693 36.85 ug/1 # 93 39) Pyrene 30.05 202 3028965 42.64 ug/1 # 92 40) Butylbenzylphthalate 32.17 149 1510210 41.23 ug/1 98 41) Benzo(a)anthracene 33.68 228 2205014 37.32 ug/1 98 42) Bis(2-ethylhexyl)phthalate 33.94 149 1941229 39.25 ug/1 95 43) Chrysene 33.81 228 2125901 36.69 ug/1 99 45) Di-n-Octylphthalate 35.67 149 3028475 43.68 ug/1 # 98 46) Benzo(b)fluoranthene 36.79 252 1781474 37.08 ug/1 # 96 47) Benzo(k)fluoranthene 36.87 252 1829755 39.06 ug/1 # 96 4 8) Benzo(a)pyrene 37.79 252 1627707 3717 ug/1 # 95 49) Indeno(1,2,3-cd)pyrene 42.15 276 1623149 /30.69 ug/1 # 93 50) Dibenz(a,h)anthracene 42.22 278 1250079 > 30.54 ug/1 # 95 51) Benzo(g,h,i)perylene 43.41 276 1315905 30 .3^ ug/1 95

(#) = qualifier out of range (m) = manual integration CAL40.D GCMS0308.M Thu Mar 21 14:44:58 2002 Page 2

NYC-WTC_000038754

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