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DEP GCMS method 608 data sheet, Feb 2002

Machine-extracted title · confidence 95%

Laboratory data sheet recording concentrations of volatile organic compounds analyzed by GCMS on February 28, 2002.

NYC-WTC_000003696–000003699

Folder label: “GCMS X 1/25/02 A 2/26/02

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NYC 9/11 Public Portal Document

* Data File C:\HPCHEM\1\DATA\FEB2 5 0 2\CAL2 5A.D Vial: 2 Acq On 26 Feb 2002 1:33 pm Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 28 11:12 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.30 168 431800 22.84 ug/1 # 87 31) 4-Bromophenyl-phenylether 24.38 248 258679 21.17 ug/1 94 32) Hexachlorobenzene 24.82 284 302661 21.15 ug/1 95 3 3) Phenanthrene 25.79 178 1355720 23.25 ug/1 99 34) Anthracene 25.93 178 1302053 22.79 ug/1 99 35) Di-n-butylphthalate 27.68 149 1761230 21.61 ug/1 99 36) Fluoranthene 29.42 202 1395949 23.98 ug/1 # 90 3 9) Pyrene 30.10 202 1422127 23.83 ug/1 # 88 40) Butylbenzylphthalate 32.22 149 722092 21.86 ug/1 97 41) Benzo(a)anthracene 33.74 228 1036788 23.77 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.99 149 956326 21.43 ug/1 97 43) Chrysene 33.87 228 1010219 23.53 ug/1 100 45) Di-n-Octylphthalate 35.73 149 1494348 —19.49 ug/1 99 46) Benzo(b)fluoranthene 36.86 252 982066 22.69 ug/1 # 97 47) Benzo(k)fluoranthene 36.94 252 1040602 23.93 ug/1 # 97 48) Benzo(a)pyrene 37.87 252 836103 23.31 ug/1 # 96 49) Indeno(1,2,3-cd)pyrene 42.28 276 959396 29.31 ug/1 # 95 50) Dibenz(a,h)anthracene 42.34 278 737897 29.49 ug/1 96 51) Benzo(g,h,i)perylene 43.55 276 792244 30.02 ug/1 94

(#) = qualifier out of range (m) = manual integration CAL25A.D GCMS0208.M Thu Feb 28 11:16:04 2002 Page 2

NYC-WTC_000003698

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NYC-WTC_000003698Source: NYC Law Department, mirrored locally

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