GCMS analysis results for sample AE02567, March 2002

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Data File : C:\HPCHEM\l\DATA\MAR1902\CAL40.D Vial: 2 Acq On : 20 Mar 2002 9:55 am Operator: Sample : new Inst : GC/MS 2 09 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 21 14:44 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.27 152 531567 20.00 ug/1 -0.08 IC) Naphthalene-d8 15.91 136 2105642 20.00 ug/1 -0.09 17) Acenaphthene -dl0 21.21 164 1130469 20.00 ug/1 -0.10 29) Phenanthrene-diO 25.67 188 1782258 20.00 ug/1 -0.10 38) Chrysene-dl2 33.74 240 1237182 20.00 ug/1 -0.11 44) Perylene-dl2 37.98 264 786836 20.00 ug/1 -0.14

System Monitoring Compounds 37) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.90 74 702101 38.93 ug/1 # 70 3) bis(2-Chloroethyl)ether 11.69 93 1105038 38.05 ug/1 90 4) 1,3-Dichlorobenzene 12.17 146 1167688 38.91 ug/1 100 5) 1,4-Dichlorobenzene 12.32 146 1181553 39.29 ug/1 99 6) 1,2-Dichlorobenzene 12.83 146 1098515 39.16 ug/1 100 7) 2,21-oxybis(1-Chloropropan 13.15 45 1533815 37.53 ug/1 99 8) N-Nitroso-di-n-propylamine 13.56 70 741285 39.24 ug/1 # 86 9) Hexachloroethane 13.68 117 445862 39.66 ug/1 100 11) Nitrobenzene 13.96 77 1096082 ' 38.08 ug/1 94 12) Isophorone 14.61 82 2075202 38.01 ug/1 99 13) bis(2-Chloroethoxy)methane 15.29 93 1347908 37.73 ug/1 97 14) 1,2,4-Trichlorobenzene 15.80 180 958365 38.77 ug/1 97 15) Naphthalene 15.97 128 3070771 39.46 ug/1 99 16) Hexachlorobutadiene 16.51 225 479240 38.89 ug/1 99 18) Hexachlorocyclopentadiene 18.70 237 407111 (53.17 ug/l 99 19) 2-Chloronaphthalene 19.48 162 1842866 37.97 ug/1 97 20) Dimethylphthalate 20.57 163 2164556 38.05 ug/1 99 21) 2,6-Dinitrotoluene 20.79 165 522484 37.84 ug/1 # 83 22) Acenaphthylene 20.75 152 2696003 38.85 ug/1 99 23) Acenaphthene 21.32 153 1866251 38.48 ug/1 98 24) 2,4-Dinitrotoluene 21.96 165 698629 37.82 ug/1 # 81 25) Diethylphthalate 22.71 149 2103696 38.09 ug/1 96 26) 4-Chlorophenyl-phenylether 22.86 204 932519 39.43 ug/1 92 27) Fluorene 22.84 166 2001570 39.02 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.33 77 2147716 36.29 ug/L # 87

(#) = qualifier out of range (m) = manual integration CAL40.D GCMS0308.M Thu Mar 21 14:44:54 2002 Page 1

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