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← Document results/DEP Box 23/GCMS X 2/25/02 A 3/23/02
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GCMS quantitation results for sample AE04033, March 2002

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Quantitation report listing response data for deuterated internal standards and surrogates from a March 29, 2002 analysis.

NYC-WTC_000038562–000038570

Folder label: “GCMS X 2/25/02 A 3/23/02”

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Data File : C:\HPCHEM\1\DATA\MAR2202\4033.D Vial: 39 Acq On : 24 Mar 2002 7:35 am Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 2 09 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 2610:212002 ।Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.27 152 492942 ' 20.00 ug/1 -0.08 10) Naphthalene-d8 15.90 136 1997726 20.00 ug/1 -0.09 17) Acenaphthene-diO 21.21 164 1108035 20.00 ug/1 -0.10 29) Phenanthrene-diO 25.65 188 1658766 20.00 ug/1 -0.11 38) Chrysene-dl2 33.72 240 1090794 20.00 ug/1 -0.12 44) Perylene-dl2 37.97 264 667573 20.00 ug/1 -0.15

System Monitoring Compounds 5,65 37) 2,4-DDD 30.73 235 82804 6.87 -ug/mL 0.23 Spiked Amount 5.000 Recovery = -137.40% /0/e Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.96 128 282 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.70 149 668 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 4033.D GCMS0308.M Tue Mar 26 10:23:24 2002 Page 1

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