Laboratory report documenting GCMS analysis of sample AE03834 for unknown compounds on March 18, 2002.
NYC-WTC_000038364–000038374Folder label: “GCMS X 2/22/02 A 2/24/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document ^UdllU L tc L 1U11 RCDOL L 21 KEVLEwE/
Data File : C:\HPCHEM\1\DATA\FEB2102\3834.D Vial: 74 Acq On : 24 Feb 2002 6:51 pm Operator: Sample : gc/ms scan 2/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 13 11:14 2002 (Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.33 152 244801 ' 20.00 ug/1 -0.03 10). Naphthalene-d8 15.97 136 945546 20.00 ug/1 -0.03 17) Acenaphthene-dlO 21.29 164 505499 20.00 ug/1 -0.03 29) Phenanthrene-dlO 25.73 188 693653 20.00 ug/1 -0.03 38) Chrysene-dl2 33.80 240 440730 20.00 ug/1 -0.04 44) Perylene-dl2 38.08 264 275550 20.00 ug/1 -0.04
System Monitoring Compounds 2.4 37) 2,4-DDD 30.81 235 48028 6.G3— ug/mL 0.31 Spiked Amount 5.000 Recovery = 132.60% 7176 Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00. 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00- 146 0 N.D. 7) 2,21 -oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.04 128 403 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene . 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.76 149 566 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. . 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 3834 .D GCMS0208.M Wed Mar 13 11:15:39 2002 Page 1
NYC-WTC_000038366
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