GCMS analysis results for sample AE04028, March 2002

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Data File : C:\HPCHEM\l\DATA\MAR2202\REFB.D Vial: 32 Acq On : 24 Mar 2002 12:40 am Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 2 09 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 268:312002 iQuant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.26 152 472952 • 20.00 ug/1 -0.09 10) Naphthalene-d8 15.91 136 1892159 20.00 ug/1 -0.09 17) Acenaphthene-diO 21.21 164 1054833 20.00 ug/1 -0.10 29) Phenanthrene-diO 25.66 188 1610382 20.00 ug/1 -0.11 38) Chrysene-di2 33.73 240 1144405 20.00 ug/1 -0.12 44) Perylene-dl2 37.98 264 731004 20.00 ug/1 -0.14

System Monitoring Compounds 37) 2,4-DDD 30.73 235 89897 7.68 ug/mL 0.24 Spiked Amount 5.000 Recovery = 153.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.91 74 85678 5.34 ug/1 # 68 3) bis(2-Chloroethyl)ether 11.66 93 214028 8.28 ug/1 92 4) 1,3-Dichlorobenzene 12.16 146 144363 5.41 ug/1 99 5) 1,4-Dichlorobenzene 12.31 146 155606 5.82 ug/1 99 6) 1,2-Dichlorobenzene 12.82 146 164005 6.57 ug/1 98 7) 2,2'-oxybis(1-Chloropropan 13.14 45 295360 8.12 ug/1 98 8) N-Nitroso-di-n-propylamine 13.53 70 147218 8.76 ug/1 # 86 9) Hexachloroethane 13.68 117 32947 3.29 ug/1 93 11) Nitrobenzene 13.94 77 193002 7.46 ug/1 93 12) Isophorone 14.59 82 437155 8.91 ug/1 100 13) bis (2-Chloroethoxy)methane 15.27 93 262497 8.18 ug/1 98 14) 1,2,4-Trichlorobenzene 15.79 180 146030 6.57 ug/1 97 15) Naphthalene 15.96 128 571128 8.17 ug/1 98 16) Hexachlorobutadiene 16.50 225 28238 2.55 ug/1 97 18) Hexachlorocyclopentadiene 18.70 237 16297 2.28 ug/1 97 19) 2-Chloronaphthalene 19.47 162 350051 7.73 ug/1 95 20) Dimethylphthalate 20.55 163 477629 9.00 ug/1 99 21) 2,6-Dinitrotoluene 20.77 165 100917 7.83 ug/1 # 81 22) Acenaphthylene 20.74 152 566399 8.75 ug/1 99 23) Acenaphthene 21.31 153 388516 8.59 ug/1 98 24) 2,4-Dinitrotoluene 21.94 165 130794 7.59 ug/1 # 77 25) Diethylphthalate 22.69 149 470545 9.13 ug/1 95 26) 4-Chlorophenyl-phenylether 22.85 204 209654 9.50 ug/1 91 27) Fluorene 22.83 166 441135 9.22 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.31 77 417316 7.56 ug/L # 85

(#) = qualifier out of range (m) = manual integration REFB.D GCMS0308.M Tue Mar 26 08:31:51 2002 Page 1

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