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GCMS analysis results for sample AE04028, March 2002

Machine-extracted title · confidence 95%

Laboratory report listing gas chromatography-mass spectrometry detection of volatile organic compounds in environmental sample AE04028.

NYC-WTC_000038494–000038501

Folder label: “GCMS X 2/25/02 A 3/23/02

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NYC 9/11 Public Portal Document yuaiic±cacion Report (Ql Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR2202\REFB.D Vial: 32 Acq On : 24 Mar 2002 12:40 am Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 268:312002 <Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.23 168 182304 8.38 ug/1 # 80 31) 4-Bromophenyl-phenylether 24.32 248 115148 9.01 ug/1 # 88 32) Hexachlorobenzene 24.75 284 131400 8.85 ug/1 # 91 33) Phenanthrene 25.72 178 632465 9.09 ug/1 98 34) Anthracene 25.85 178 602990 8.74 ug/1 98 35) Di-n-butylphthalate 27.62 149 807152 9.22 ug/1 99 36) Fluoranthene 29.35 202 643850 8.82 ug/1 # 94 39) Pyrene 30.03 202 664964 10.12 ug/1 # 93 40) Butylbenzylphthalate 32.16 149 301193 8.89 ug/1 # 98 41) Benzo(a)anthracene 33.66 228 479000 8.76 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.93 149 432604 9.46 ug/1 95 43) Chrysene 33.79 228 502238 9.37 ug/1 99 45) Di-n-Octylphthalate 35.67 149 494576 7.68 ug/1 # 98 46) Benzo(b)fluoranthene 36.77 252 399958m 8.96 ug/1 47) Benzo(k)fluoranthene 36.85 252 429338 9.86 ug/1 99 48) Benzo(a)pyrene 37.78 252 314204 7.72 ug/1 97 49) Indeno(1,2,3-cd)pyrene 42.11" 276 319032 6.49 ug/1 96 50) Dibenz(a,h)anthracene 42.19 278 272503 7.16 ug/1 96 51) Benzo(g,h,i)perylene 43.36 276 270953 6.76 ug/1 94

(#) = qualifier out of range (m) = manual integration REFB.D GCMS0308.M Tue Mar 26 08:31:54 2002 Page 2

NYC-WTC_000038500

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NYC-WTC_000038500Source: NYC Law Department, mirrored locally

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