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GCMS reference analysis results for organic contaminants, March 2002

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Reference data report displaying measured concentrations and detection limits for target analytes analyzed on March 21, 2002.

NYC-WTC_000010289–000010296

Folder label: “GCMS X 1/27/02 A 2/26/02 - 3/5/02 3/20/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR1902\REF2.D Vial: 5 Acq On : 20 Mar 2002 3:04 am Operator : Sample : gc/ms scan 3/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 218:362002 ।Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.23 168 203628 7.17 ug/1 # 84 31) 4-Bromophenyl-phenylether 24.31 248 124770 7.47 ug/1 95 32) Hexachlorobenzene 24.75 284 139566 7.20 ug/1 92 3 3) Phenanthrene 25.73 178 726968 8.00 ug/1 99 34) Anthracene 25.85 178 693332 7.69 ug/1 99 35) Di-n-butylphthalate 27.63 149 963769 8.43 ug/1 99 36) Fluoranthene 29.34 202 745267 7.82 ug/1 # 90 3 9) Pyrene 30.02 202 779158 9.09 ug/1 # 89 40) Butylbenzylphthalate 32.15 149 377832 8.55 ug/1 97 41) Benzo(a)anthracene 33.67 228 576812 8.09 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.92 149 522874 8.76 ug/1 96 43) Chrysene 33.80 228 600748 8.59 ug/1 100 45) Di-n-Octylphthalate 35.67 149 731381 8.22 ug/1 # 98 46) Benzo(b)fluoranthene 36.77 252 513889 8.33 ug/1 # 95 47) Benzo(k)fluoranthene 36.84 252 511370 8.51 ug/1 # 96 4 8) Benzo(a)pyrene 37.77 252 402841 7.17 ug/1 # 96 49) Indeno (1,2,3-cd) pyrene 42.10 276 472248 6.96 ug/1 95 50) Dibenz(a,h)anthracene 42.18 278 403987 7.69 ug/1 # 94 51) Benzo(g,h,i)perylene 43.35 276 403736 7.29 ug/1 # 93

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0308.M Thu Mar 21 08:39:48 2002 Page 2

NYC-WTC_000010292

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NYC-WTC_000010292Source: NYC Law Department, mirrored locally

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