GCMS calibration table for polycyclic aromatic hydrocarbons, January 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\JAN1502\CAL10.D Vial: 2 Acq On 15 Jan 2002 9:19 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Feb 4 12:42 2002 Quant Results File: GCMS1126.RES

Quant Method : ■ C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq« Meth : GCMS0103

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.51 152 788874 20.00 ug/1 -0.19 10) Naphthalene-d8 15.10 136 3059834 20.00 ug/1 -0.21 17) Acenaphthene-diO 20.36 164 1537098 20.00 ug/1 -0.22 . 29) Phenanthrene-diO 24.77 188 2110629 20.00 ug/1 -0.22 38) Chrysene-dl2 32.81 240 1118804 20.00 ug/1 -0.23 44) Perylene-dl2 36.86 264 668791 20.00 ug/1 -0.26

System Monitoring Compounds 37) 2,4-DDD 0.00 235 Od 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.27 74 375062 10.81 ug/1 95 3) bis(2-Chloroethyl)ether 10.95 93 630014 11.57 ug/1 99 4) 1,3-Dichlorobenzene 11.40 146 566433 9.87 ug/1 99 5) 1,4-Dichlorobenzene 11.54 146 577934 9.96 ug/1 99 6) 1,2-Dichiorobenzene 12.05 146 542689 10.14 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 12.40 45 962144 ug/1 100 8) N-Nitroso-di-n-propylamine 12.78 70 403737 ug/1 97 9) Hexachloroethane 12.88 117 237293 11.25 ug/1 98 11) Nitrobenzene 13.18 77 610031 12.79 ug/1 98 12) 1sophorone 13.82 82 1096657 11.94 ug/1 99 13) bis(2-Chloroethoxy)methane 14.52 93 702121 11.37 ug/1 100 14) 1,2,4-Trichlorobenzene 14.99 180 439440 9.89 ug/1 98 15) Naphthalene 15.15 128 1512464 10.34 ug/1 99 16) Hexachiorobutadiene 15.70 225 229841 10.62 ug/1 98 18) Hexachlorocyclopentadiene 17.88 237 56357 5.09 ug/1 97 19) 2-Chloronaphthalene 18.63 162 835269 9.53 ug/1 99 20) Dimethylphthalate 19.75 163 984255 9.64 ug/1 100 21) 2,6-Dinitrotoluene 19.96 165 219614 9.10 ug/1 99 22) Acenaphthylene 19.89 152 1252155 10.16 ug/1 99 23) Acenaphthene 20.45 153 874074 9.92 ug/1 100 24) 2,4-Dinitrotoluene 21.12 165 272577 8.88 ug/1 96 25) Diethylphthalate 21.88 149 996908 10.55 ug/1 99 26) 4-Chlorophenyl-phenylether 22.00 204 410480 9.95 ug/1 97 27) Fluorene 21.96 166 893932 9.89 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 22.47 77 1117503 11.44 ug/L 96

(#) = qualifier out of range (m) = manual integration CAL10.D GCMS1126.M Wed Feb 06 12:42:26 2002 Page 1

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