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GCMS calibration table for polycyclic aromatic hydrocarbons, January 2002

Machine-extracted title · confidence 90%

Calibration report showing retention times and response factors for deuterated internal standards used in PAH analysis.

NYC-WTC_000016065–000016067

Folder label: “GCMS X 12/26/01 A 1/15-1/16/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\ JANI502\CAL10.D Vial: 2 Acq On 15 Jan 2002 9:19 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Feb 4 12:42 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.40 168 379399 10.12 ug/1 98 31) 4-Bromophenyl-phenylether 23.46 248 211797 10.20 ug/1 100 32) Hexachlorobenzene 23.87 284 255095 11.17 ug/1 96 3 3) Phenanthrene 24.84 178 1151980 10.31 ug/1 99 34) Anthracene 24.97 178 1121819 10.07 ug/1 100 35) Di-n-butylphthalate 26.80 149 1619539 10.89 ug/1 100 3 6) Fluoranthene 28.44 202 1057421 9.80 ug/1 99 3 9) Pyrene 29.11 202 1072514 11.11 ug/1 99 40) Butylbenzylphthalate 31.30 149 555334 11.01 ug/1 97 41) Benzo(a)anthracene 32.75 228 630029 9.45 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.10 149 728079 10.68 ug/1 100 43) Chrysene 32.87 228 629314 9.63 ug/1 98 45) Di-n-Octylphthalate 34.84 149 913332 10.28 ug/1 96 46) Benzo(b)fluoranthene 35.83 252 503290 10.00 ug/1 99 47) Benzo(k)fluoranthene 35.89 252 568522 11.01 ug/1 98 48) Benzo(a)pyrene 36.70 252 422041 9.65 ug/1 98 49) Indeno(l,2,3-cd)pyrene 40.42 276 413675 9.46 ug/1 95 50) Dibenz(a,h)anthracene 40.47 278 316386 9.24 ug/1 96 51) Benzo(g,h,i)perylene 41.46 276 359587 9.62 ug/1 99

(#) = qualifier out of range (m) = manual integration CAL10.D GCMS1126.M Wed Feb 06 12:42:31 2002 Page 2

NYC-WTC_0000 16066

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NYC-WTC_000016066Source: NYC Law Department, mirrored locally

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