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GCMS calibration data for sample AD29926, Jan 2002

Machine-extracted title · confidence 100%

Calibration records for gas chromatography mass spectrometry analysis of volatile organic compounds in environmental samples.

NYC-WTC_000037375–000037378

Folder label: “GCMS X 12/11/01 A 12/16/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC14O1\CAL25B. D Vial: 2 Acq On 16 Dec 2001 4:49 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 30 9:30 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Jan 25 15:57:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.63 168 2683639m 24.95 ug/1 31) 4-Bromophenyl-phenylether 23.67 248 1471054 24.68 ug/1 94 32) Hexachlorobenzene 24.09 284 1645249 25.10 ug/1 96 3 3) Phenanthrene 25.07 178 7784654 24.26 ug/1 99 34) Anthracene 25.20 178 7688965 24.04 ug/1 99 35) Di-n-butylphthalate 27.00 149 10431604 24.43 ug/1 99 3 6) Fluoranthene 28.68 202 7894155 25.48 ug/1 98 39) Pyrene 29.34 202 8008568 22.61 ug/1 98 40) Butylbenzylphthalate 31.51 149 4215697 22.79 ug/1 94 41) Benzo(a)anthracene 32.99 228 6017570 24.61 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.30 149 5410966 21.65 ug/1 96 43) Chrysene 33.12 228 5694244 23.75 ug/1 100 45) Di-n-Octylphthalate 35.04 149 8562985 22.62 ug/1 96 4 6) Benzo(b)fluoranthene 36.06 252 5522896 25.77 ug/1 98 47) Benzo(k)fluoranthene 36.14 252 5538311 25.18 ug/1 98 48) Benzo(a)pyrene 36.96 252 4602194 24.70 ug/1 99 49) Indeno(1,2,3-cd)pyrene 40.83 276 4421209 23.73 ug/1 100 50) Dibenz(a,h)anthracene 40.89 278 3476322 23.83 ug/1 99 51) Benzo(g,h,i)perylene 41.94 276 3554115 22.32 ug/1 98

*

(#) = qualifier out of range (m) = manual integration CAL25B.D GCMS1126.M Wed Jan 30 09:31:50 2002 Page 2

NYC-WTC_000037377

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NYC-WTC_000037377Source: NYC Law Department, mirrored locally

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