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GCMS extraction method log, Dec 2001

Machine-extracted title · confidence 85%

Laboratory record documenting the extraction method parameters for sample AD29229 analyzed in December 2001.

NYC-WTC_000036201–000036204

Folder label: “GCMS X 12/4/01 A 12/10/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) 5 Data File C:\HPCHEM\l\DATA\DEC1001\CAL40.D Vial: 2 Acq On 10 Dec 2001 10:43 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 12 15:21 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.62 168 1895513 35.87 ug/1 94 31) 4-Bromophenyl-phenylether 23.67 248 1115609 38.10 ug/1 98 3 2) Hexachlorobenzene 24.09 284 1223654 38.00 ug/1 97 3 3) Phenanthrene 25.06 178 5782827 36.68 ug/1 98 3 4) Anthracene 25.19 178 5679789 36.14 ug/1 99 35) Di-n-butylphthalate 27.00 149 7961481 37.95 ug/1 99 36) Fluoranthene 28.67 202 5968096 39.22 ug/1 98 3 9) Pyrene 29.34 202 6045206 35.15 ug/1 98 40) Butylbenzylphthalate 31.51 149 3246774 36.14 ug/1 95 41) Benzo(a)anthracene 32.98 228 4507107 37.96 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.30 149 4287223 35.32 ug/1 100 43) Chrysene 33.11 228 4291750 36.86 ug/1 99 45) Di-n-Octylphthalate 35.04 149 6800598 36.84 ug/1 # 97 46) Benzo(b)fluoranthene 36.06 252 3937219 37.67 ug/1 99 47) Benzo(k)fluoranthene 36.13 252 3703098 34.52 ug/1 98 48) Benzo(a)pyrene 36.95 252 3450571 37.97 ug/1 100 4 9) Indeno(1,2,3 -cd)pyrene 40.82 276 3579446 39.39 ug/1 99 5 0) Dibenz(a,h)anthracene 40.88 278 2791533 39.23 ug/1 98 51) Benzo(g,h,i)perylene 41.93 276 2948471 37.98 ug/1 96

(#) = qualifier out of range (m) = manual integration CAL40.D GCMS1126.M Fri Dec 21 09:29:10 2001 Page 2

NYC-WTC_000036203

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NYC-WTC_000036203Source: NYC Law Department, mirrored locally

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