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GCMS calibration log sample AD29289, Dec 2001

Machine-extracted title · confidence 90%

Calibration log for GCMS analysis of sample AD29289 listing target analytes and detection limits.

NYC-WTC_000036341–000036344

Folder label: “GCMS X 12/5/01 A 12/12/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\ 1\DATA\DEC12 01\CAL4 0.D Vial: 2 Acq On 12 Dec 2001 11:46 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 12 14:21 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.64 168 3303372 35.96 ug/1 94 31) 4-Bromophenyl-phenylether 23.68 248 1866184 36.66 ug/1 99 32) Hexachlorobenzene 24.10 284 2053420 36.68 ug/1 97 3 3) Phenanthrene 25.07 178 9654155 35.23 ug/1 99 3 4) Anthracene 25.21 178 9375217 34.32 ug/1 99 35) Di-n-butylphthalate 27.01 149 13113830 35.96 ug/1 99 36) Fluoranthene 28.69 202 10036775 37.94 ug/1 100 3 9) Pyrene 29.35 202 10128656 34.27 ug/1 99 40) Butylbenzylphthalate 31.52 149 5498243 35.62 ug/1 95 41) Benzo(a)anthracene 32.99 228 7660813 37.55 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.31 149 7027565 33.69 ug/1 100 43) Chrysene 33.12 228 7200766 35.99 ug/1 99 45) Di-n-Octylphthalate 35.05 149 11139302 34.85 ug/1 # 98 46) Benzo(b)fluoranthene 36.07 252 6823535 37.71 ug/1 99 47) Benzo(k)fluoranthene 36.14 252 6734929m 36.27 ug/1 48) Benzo(a)pyrene 36.97 252 5874046 37.34 ug/1 99 49) Indeno(l,2,3-cd)pyrene 40.84 276 6266283 39.83 ug/1 99 50) Dibenz(a,h)anthracene 40.91 278 4891836 39.71 ug/1 98 51) Benzo(g,h,i)perylene 41.95 276 5111128 38.03 ug/1 95

(#) = qualifier out of range (m) = manual integration CAL40.D GCMS1126.M Thu Dec 27 12:22:41 2001 Page 2

NYC-WTC_000036343

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NYC-WTC_000036343Source: NYC Law Department, mirrored locally

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