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GCMS calibration results for sample AD29024, Dec 18 2001

Machine-extracted title · confidence 95%

Calibration data sheet verifying instrument response for nitrosamines and benzene derivatives.

NYC-WTC_000035900–000035903

Folder label: “GCMS X 11/30/01 A 12/11/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C: \HPCHEM\ 1 \DATA\DEC10 01 \CAL4 0A. D Vial: 2 Acq On 11 Dec 2001 10:07 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 18 11:11 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.63 168 2863159 37.11 ug/1 94 31) 4-Bromophenyl-phenylether 23.67 248 1580016 36.96 ug/1 97 3 2) Hexachlorobenzene 24.10 284 1733945 36.88 ug/1 98 3 3) Phenanthrene 25.08 178 8176268 35.52 ug/1 99 3 4) Anthracene 25.20 178 8064402 35.15 ug/1 100 35) Di-n-butylphthalate 27.00 149 10957500 35.78 ug/1 99 36) Fluoranthene 28.68 202 8495312 38.24 ug/1 99 3 9) Pyrene 29.35 202 8696314 34.26 ug/1 98 40) Butylbenzylphthalate 31.51 149 4594629 34.65 ug/1 94 41) Benzo(a)anthracene 32.99 228 6578283 37.54 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.30 149 5918617 33.04 ug/1 100 43) Chrysene 33.13 228 6260836 36.43 ug/1 99 45) Di-n-Octylphthalate 35.05 149 9580783 34.31 ug/1 # 97 46) Benzo(b)fluoranthene 36.07 252 6066028 38.37 ug/1 99 47) Benzo(k)fluoranthene 36.15 252 5290676 32.60 ug/1 99 48) Benzo(a)pyrene 36.96 252 5149503 37.46 ug/1 100 49) Indeno(l,2,3-cd)pyrene 40.84 276 5474320 39.82 ug/1 98 50) Dibenz(a,h)anthracene 40.90 278 4284787 39.81 ug/1 98 51) Benzo(g,h,i)perylene 41.95 276 4471310 38.07 ug/1 96

(#) = qualifier out of range (m) = manual integration CAL40A.D NP091101.M Tue Dec 18 11:12:13 2001 Page 2

NYC-WTC_000035902

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NYC-WTC_000035902Source: NYC Law Department, mirrored locally

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