GCMS calibration results for sample AD29024, Dec 18 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC1001\CAL40A.D Vial: 2 Acq On 11 Dec 2001 10:07 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 18 11:11 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.68 152 1512101 20.00 ug/1 -0.02 10) Naphthalene-d8 15.30 136 5837449 20.00 ug/1 0.00 17) Acenaphthene-diO 20.57 164 2721852 20.00 ug/1 0.00 29) Phenanthrene-diO 24.99 188 4345996 20.00 ug/1 0.00 38) Chrysene-dl2 33.03 240 2941109 20.00 ug/1 0.00 44) Perylene-dl2 37.13 264 2101701 20.00 ug/1 0.01

System Monitoring Compounds 37) 2,4-DDD 30.06 235 254 0.00 ug/mL 0.00 Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.40 74 2945224m 44.29 ug/1 3) bis(2-Chloroethyl)ether 11.13 93 4104047 39.32 ug/1 98 4) 1,3-Dichlorobenzene 11.58 146 4146421 37.71 ug/1 100 5) 1,4-Dichlorobenzene 11.73 146 4129825 37.14 ug/1 99 6) 1,2-Dichlorobenzene 12.24 146 3706237 36.14 ug/1 98 7) 2,2* -oxybis(1-Chloropropan 12.58 45 5521233 41.54 ug/1 97 8) N-Nitroso-di-n-propylamine 13.00 70 2488916 41.86 ug/1 98 9) Hexachloroethane 13.07 117 1600288 39.56 ug/1 98 11) Nitrobenzene 13.38 77 3728070 40.98 ug/1 99 12) 1sophorone 14.03 82 7125006 40.65 ug/1 98 13) bis(2-Chloroethoxy)methane 14.71 93 4660963 39.58 ug/1 100 14) 1,2,4-Trichlorobenzene 15.19 180 3186744 37.60 ug/1 99 15) Naphthalene 15.35 128 10284733 36.87 ug/1 100 16) Hexachiorobutadiene 15.89 225 1553173 37.60 ug/1 99 18) Hexachlorocyclopentadiene 18.07 237 712919 36.36 ug/1 98 19) 2-Chloronaphthalene 18.84 162 6046188 38.94 ug/1 98 20) Dimethylphthalate 19.97 163 7137990 39.46 ug/1 100 21) 2,6-Dinitrotoluene 20.18 165 1777382m 41.58 ug/1 22) Acenaphthylene 20.10 152 8470471 38.82 ug/1 99 2 3) Acenaphthene 20.68 153 5878090 37.67 ug/1 100 24) 2,4-Dinitrotoluene 21.35 165 2325460 42.80 ug/1 # 90 25) Diethylphthalate 22.11 149 6639000 39.66 ug/1 99 26) 4-Chlorophenyl-phenylether 22.22 204 2696637 36.90 ug/1 100 27) Fluorene 22.19 166 5867404 36.64 ug/1 100 2 8) Azobenzen/ 1,2-Diphenylhyd 22.69 77 7356246 42.53 ug/L 97

(#) = qualifier out of range (m) = manual integration CAL40A.D NP091101.M Tue Dec 18 11:12:11 2001 Page 1

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