GCMS blank analysis results, sample AD29135, Dec 2001

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Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\DEC1001\CAL40.D Vial: 2 Acq On 10 Dec 2001 10:43 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 12 15:21 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.68 152 1036642 20.00 ug/1 -0.02 10) Naphthalene-d8 15.29 136 4027469 20.00 ug/1 -0.02 17) Acenaphthene-diO 20.57 164 1929138 20.00 ug/1 -0.01 2 9) Phenanthrene-dl0 24.99 188 2976834 20.00 ug/1 0.00 38) Chrysene-dl2 33.03 240 1992746 20.00 ug/1 0.00 44) Perylene-dl2 37.12 264 1389287 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 29.90 235 18250 0.51 ug/mL -0.17 Spiked Amount 5.000 Recovery = 10.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.40 74 1928764m 42.30 ug/1 3) bis(2-Chloroethyl)ether 11.12 93 2847377 39.79 ug/1 98 4) 1,3-Dichlorobenzene 11.58 146 2891850 38.36 ug/1 100 5) 1,4-Dichlorobenzene 11.72 146 2901268 38.06 ug/1 99 6) 1,2-Dichlorobenzene 12.23 146 2629349 37.40 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 12.57 45 3839461 42.13 ug/1 99 8) N-Nitroso-di-n-propylamine 12.98 70 1709985 41.95 ug/1 97 9) Hexachloroethane 13.06 117 1096166 39.53 ug/1 98 11) Nitrobenzene 13.37 77 2623852 41.80 ug/1 98 12) Isophorone 14.02 82 4911986 40.61 ug/1 97 13) bis(2-Chloroethoxy)methane 14.70 93 3201919 39.41 ug/1 100 14) 1,2,4-Trichlorobenzene 15.18 180 2219853 37.96 ug/1 98 15) Naphthalene 15.35 128 7300815 37.94 ug/1 99 16) Hexachiorobutadiene 15.88 225 1098418 38.54 ug/1 100 18) Hexachlorocyclopentadiene 18.07 237 380608 .39 ug/1 99 19) 2-Chloronaphthalene 18.84 162 4221055 38.35 ug/1 98 20) Dimethylphthalate 19.96 163 5015822 39.12 ug/1 100 21) 2,6-Dinitrotoluene 20.17 165 1247223 41.17 ug/1 # 66 22) Acenaphthylene 20.10 152 5898222 38.13 ug/1 99 2 3) Acenaphthene 20.67 153 4198659 37.97 ug/1 100 24) 2,4-Dinitrotoluene 21.34 165 1576452 40.93 ug/1 # 89 25) Diethylphthalate 22.10 149 4709796 39.70 ug/1 99 26) 4-Chlorophenyl-phenylether 22.21 204 1953038 37.71 ug/1 96 2 7) Fluorene 22.18 166 4247881 37.43 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 22.69 77 5176489 42.23 ug/L 98

(#) = qualifier out of range (m) = manual integration CAL40.D GCMS1126.M Wed Dec 12 15:22:21 2001 Page 1

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