GCMS calibration data for sample AD29926, Jan 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC14 01\CAL2 5B.D Vial: 2 Acq On 16 Dec 2001 4:49 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 30 9:30 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Jan 25 15:57:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.68 152 2095465 20.00 ug/1 -0.02 10) Naphthalene-d8 15.30 136 8125514 20.00 ug/1 -0.01 17) Acenaphthene-diO 20.57 164 3833713 20.00 ug/1 -0.01 29) Phenanthrene-diO 25.00 188 6059467 20.00 ug/1 0.00 38) Chrysene-dl2 33.04 240 4103354 20.00 ug/1 0.00 44) Perylene-d12 37.13 264 2848865 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 0.00 235 Od 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.40 74 2702028 29.32 ug/1 87 3) bis(2-Chloroethyl)ether 11.13 93 3909023 27.02 ug/1 95 4) 1,3-Dichlorobenzene 11.58 146 3780485 24.81 ug/1 99 5) 1,4-Dichlorobenzene 11.73 146 3757918 24.38 ug/1 98 6) 1,2-Dichlorobenzene 12.24 146 3385832 23.82 ug/1 100 7) 2,2'-oxybi s(1-Chloropropan 12.57 45 5671900 0.79 ug/1 100 8) N-Nitroso-di-n-propylamine 12.99 70 2469987 9.97 ug/1 95 9) Hexachloroethane 13.07 117 1501979 26.80 ug/1 95 11) Nitrobenzene 13.38 77 3649038 28.81 ug/1 92 12) Isophorone 14.03 82 6966071 28.55 ug/1 97 13) bis(2-Chloroethoxy)methane 14.71 93 4500345 27.45 ug/1 99 14) 1,2,4-Trichlorobenzene 15.19 180 2957583 25.07 ug/1 99 15) Naphthalene 15.35 128 9693413 24.97 ug/1 100 16) Hexachlorobutadiene 15.88 225 1451717 25.25 ug/1 100 18) Hexachlorocyclopentadiene 18.07 237 604013 21.87 ug/1 99 19) 2-Chloronaphthalene 18.84 162 5669724 25.92 ug/1 97 20) Dimethylphthalate 19.97 163 6628206 26.02 ug/1 100 21) 2,6-Dinitrotoluene 20.18 165 1635213 27.16 ug/1 # 86 2 2) Acenaphthylene 20.10 152 7957601 25.89 ug/1 100 23) Acenaphthene 20.67 153 5533743 25.18 ug/1 99 24) 2,4-Dinitrotoluene 21.35 165 2121942 27.72 ug/1 # 86 25) Diethylphthalate 22.11 149 6245325 26.49 ug/1 99 26) 4-Chlorophenyl-phenylether 22.21 204 2617565 25.43 ug/1 96 27) Fluorene 22.18 166 5637915 25.00 ug/1 99 2 8) Azobenzen/ 1,2-Diphenylhyd 22.69 77 7313573 30.02 ug/L 95

(#) = qualifier out of range (m) = manual integration CAL25B.D GCMS1126.M Wed Jan 30 09:31:47 2002 Page 1

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