DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC2 7 01\ CAL4 0.D Vial: 2 Acq On 29 Dec 2001 6:41 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 24 14:05 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.68 152 856488 20.00 ug/1 -0.02 10) Naphthalene-d8 15.29 136 3332855 20.00 ug/1 -0.02 17) Acenaphthene-diO 20.57 164 1585432 20.00 ug/1 -0.01 29) Phenanthrene-diO 24.99 188 2391078 20.00 ug/1 0.00 38) Chrysene-dl2 33.03 240 1603161 20.00 ug/1 0.00 44) Perylene-dl2 37.12 264 1010761 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 0.00 235 Od 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds 32 0 Qvalue 2) N-nitroso-dimethyl amine 5.44 74 1740146 46.20 ug/1 99 3) bis(2-Chloroethyl)ether 11.12 93 2528103 42.76 ug/1 100 4) 1,3-Dichlorobenzene 11.58 146 2427237 38.97 ug/1 100 5) 1,4-Dichlorobenzene 11.72 146 2459858 3 9.05 ug/1 98 6) 1,2-Dichlorobenzene 12.24 146 2258157 38.87 ug/1 98 7) 2,21-oxybis(1-Chloropropan 12.57 45 3925273 /52.14ug/l 99 8) N-Nitroso-di-n-propylamine 12.98 70 1702778 <50.56/ug/1 99 9) Hexachloroethane 13.06 117 1009352 44.06 ug/1 99 11) Nitrobenzene 13.37 77 2580520 (49.68 ug/1 100 12) Is ophorone 14.02 82 4595235 45. 91 ug/1 99 13) bis(2-Chloroethoxy)methane 14.70 93 2924759 43.50 ug/1 100 14) 1,2,4-Trichlorobenzene 15.18 180 1865036 38.54 ug/1 99 15) Naphthalene 15.35 128 6349429 39.87 ug/1 99 16) Hexachlorobutadiene 15.88 225 963395 4085 ug/1 99 18) Hexachlorocyclopentadiene 18.07 237 340053 C2977ug/1 100 19) 2-Chloronaphthalene 18.84 162 3564220 39.41 ug/1 98 20) Dimethylphthalate 19.96 163 4139196 39.28 ug/1 100 21) 2,6-Dinitrotoluene 20.17 165 980304 39.38 ug/1 96 22) Acenaphthylene 20.10 152 5026529 39.54 ug/1 99 2 3) Acenaphthene 20.67 153 3599632 39.60 ug/1 100 24) 2,4-Dinitrotoluene 21.34 165 1258040 39.75 ug/1 97 25) Diethylphthalate 22.09 149 4111759 42.17 ug/1 100 26) 4-Chlorophenyl-phenylether 22.21 204 1707543 40.12 ug/1 99 27) Fluorene 22.18 166 3703401 39.71 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 22.69 77 4684085 46.50 ug/L 100

(#) = qualifier out of range (m) = manual integration CAL40.D GCMS1126.M Thu Jan 24 14:07:20 2002 Page 1

NYC-WTC_000004177