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GCMS calibration results for sample AD30705, Jan 2002

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Laboratory report documenting GCMS calibration data for sample AD30705 conducted on January 2, 2002.

NYC-WTC_000018579–000018582

Folder label: “GCMS X 12/19/01 A 1/2/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC3101\CAL4 0B.D Vial: 2 Acq On 2 Jan 2002 12:25 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 25 9:22 2002 Quant Results File: GCMS1126.RES

Quant Method.: C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title ': 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.62 168 2191727 39.41 ug/1 95 31) 4-Bromophenyl-phenylether 23.67 248 1194152 38.75 ug/1 98 32) Hexachlorobenzene 24.09 284 1363135 40.23 ug/1 97 33) Phenanthrene 25.07 178 6408145 38.63 ug/1 100 3 4) Anthracene 25.20 178 6199637 37.49 ug/1 99 35) Di-n-butylphthalate 27.00 149 8862766 40.15 ug/1 100 36) Fluoranthene 28.68 202 6463407 40.36 ug/1 98 39) Pyrene 29.35 202 6560358 36.17 ug/1 98 4 0) Butylbenzylphthalate 31.51 149 3546720 37.44 ug/1 100 41) Benzo(a)anthracene 32.99 228 4727368 37.76 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.30 149 4534169 35.42 ug/1 98 43) Chrysene 33.12 228 4655600 37.92 ug/1 100 45) Di-n-Octylphthalate 35.04 149 7065979 39.51 ug/1 100 46) Benzo(b)fluoranthene 36.07 252 3800021 37.53 ug/1 100 47) Benzo(k)fluoranthene 36.14 252 4118636 39.64 ug/1 99 48) Benzo(a)pyrene 36.96 252 3394180 38.56 ug/1 99 49) Indeno(1,2,3-cd) pyrene 40.84 276 3274132 37.20 ug/1 99 50) Dibenz(a,h)anthracene 40.89 278 2583765 37.49 ug/1 100 51) Benzo(g,h,i)perylene 41.94 276 2632162 35.00 ug/1 99

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(#) = qualifier out of range (m) = manual integration CAL40B.D GCMS1126.M Fri Jan 25 09:25:53 2002 Page 2

NYC-WTC_0000 18581

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NYC-WTC_000018581Source: NYC Law Department, mirrored locally

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