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GCMS calibration results for sample AD30694, Jan 2002

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Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.

NYC-WTC_000018060–000018063

Folder label: “GCMS X 12/27/01 A 1/16/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C: \HPCHEM\ 1 \DATA\DEC3101 \CAL4 0A. D Vial: 2 Acq On 1 Jan 2002 12:12 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 18 8:38 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update • : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.63 168 2010725 40.62 ug/1 # 87 31) 4-Bromophenyl-phenylether 23.66 248 1061967 38.72 ug/1 93 32) Hexachlorobenzene 24.10 284 1214140 40.25 ug/1 98 3 3) Phenanthrene 25.07 178 5783221 39.16 ug/1 98 34) Anthracene 25.20 178 5618974 38.17 ug/1 99 35) Di-n-butylphthalate 27.01 149 7831996 39.86 ug/1 # 99 36) Fluoranthene 28.68 202 5759517 40.41 ug/1 97 39) Pyrene . 29.35 202 5851940 36.88 ug/1 98 40) Butylbenzylphthalate 31.51 149 3042616 36.71 ug/1 88 41) Benzo(a)anthracene 32.98 228 4161454 37.99 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.30 149 3846517 34.35 ug/1 98 43) Chrysene 33.12 228 4083779 38.02 ug/1 99 45) Di-n-Octylphthalate 35.05 149 5788826 38.43 ug/1 # 94 46) Benzo(b)fluoranthene 36.07 252 3387137 39.71 ug/1 99 47) Benzo(k)fluoranthene 36.13 252 3329763 38.04 ug/1 100 4 8) Benzo(a)pyrene 36.96 252 2891526 38.99 ug/1 98 49) Indeno(1,2,3-cd)pyrene 40.83 276 2731604 36.84 ug/1 96 50) Dibenz(a,h)anthracene 40.89 278 2139328 36.84 ug/1 96 51) Benzo(g,h,i)perylene 41.93 276 2190768 34.58 ug/1 93

(#) = qualifier out of range (m) = manual integration CAL40A.D GCMS1126.M Fri Jan 18 08:39:22 2002 Page 2

NYC-WTC_0000 18062

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NYC-WTC_000018062Source: NYC Law Department, mirrored locally

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