GCMS calibration results for sample AD30694, Jan 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC3101\CAL4 0A.D Vial: 2 Acq On 1 Jan 2002 12:12 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 18 8:38 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.68 152 1027033 20.00 ug/1 -0.01 10) Naphthalene-d8 15.29 136 3903066 20.00 ug/1 -0.01 17) Acenaphthene-diO 20.56 164 1855130 20.00 ug/1 -0.01 29) Phenanthrene-diO 24.99 188 2788272 20.00 ug/1 0.00 38) Chrysene-dl2 33.04 240 1838350 20.00 ug/1 0.00 44) Perylene-dl2 37.12 264 1133787 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 0.00 235 Od 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.43 74 2023845m 44.80 ug/1 3) bis(2-Chloroethyl)ether 11.12 93 3125129 44.08 ug/1 92 4) 1,3-Dichlorobenzene 11.58 146 2900590 38.83 ug/1 99 5) 1,4-Dichlorobenzene 11.73 146 2925511 38.73 ug/1 99 6) 1,2-Dichlorobenzene 12.24 146 2693451 38.67 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 12.57 45 4695735 (52201 ug/1 97 8) N-NitrosO-di-n-propylamine 12.99 70 2018721 49.98 ug/1 91 9) Hexachloroethane 13.06 117 1202857 43.78 ug/1 89 11) Nitrobenzene . 13.37 77 3072246 50250 ug/1 88 12) 1sophorone 14.02 82 5493489 46.87 ug/1 # 93 13) bis(2-Chloroethoxy)methane 14.70 93 3512913 44.61 ug/1 99 14) 1,2,4-Trichlorobenzene 15.18 180 2203702 38.88 ug/1 98 15) Naphthalene 15.35 128 7428007 39.83 ug/1 100 16) Hexachlorobutadiene 15.89 225 1125182 40.74 ug/1 99 18) Hexachlorocyclopentadiene 18.06 237 439479 32.88 ug/1 98 19) 2-Chloronaphthalene 18.84 162 4179163 39.49 ug/1 95 20) Dimethylphthalate 19.96 163 4822757 39.12 ug/1 100 21) 2,6-Dinitrotoluene 20.18 165 1157785 39.74 ug/1 # 60 22) Acenaphthylene 20.10 152 5847036 39.31 ug/1 100 2 3) Acenaphthene 20.66 153 4176428 39.27 ug/1 99 24) 2,4-Dinitrotoluene 21.34 165 1506485 40.68 ug/1 # 78 25) Diethylphthalate 22.09 149 4770473 41.82 ug/1 98 26) 4-Chlorophenyl-phenylether 22.21 204 1964197 39.44 ug/1 94 27) Fluorene 22.19 166 4295266 39.36 ug/1 98 28) Azobenzen/ 1,2-Diphenylhyd" 22.68 77 5999970 (5090 ug/L # 89

(#) = qualifier out of range (m) = manual integration CAL40A.D GCMS1126.M Fri Jan 18 08:39:18 2002 Page 1

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