NYC-WTC_000017654
Document showing calibration results for GCMS analysis of volatile organic compounds on December 27, 2001.
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GCMS calibration results for volatile compounds, Jan 2002
Machine-extracted title · confidence 90%Calibration report for gas chromatography-mass spectrometry analysis of nitrosamines and chlorinated benzenes conducted on December 22, 2001.
NYC-WTC_000019040–000019043Folder label: “GCMS X 12/13/01 A 12/22/01 AND 12/27/01”
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\1\DATA\DEC2101\CAL4 0A.D Vial: 2 Acq On 22 Dec 2001 7:50 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 22 8:39 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title .: 209 625/TCLP calibration table Last Update ': Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Compound R.T. Qlon Response Cone Unit Qvalue
30) N-Nitrosodiphenylamine 22.63 168 2990511 38.01 ug/1 # 88 31) 4-Bromophenyl-phenylether 23.68 248 1661974 38.13 ug/1 100 3 2) Hexachlorobenzene 24.10 284 1867687 38.96 ug/1 99 3 3) Phenanthrene 25.07 178 8813147 37.55 ug/1 99 3 4) Anthracene 25.21 178 8473851 36.23 ug/1 99 35) Di-n-butylphthalate 27.01 149 11935896 38.22 ug/1 99 3 6) Fluoranthene 28.68 202 9057241 39.98 ug/1 95 3 9) Pyrene 29.35 202 9226131 34.78 ug/1 99 40) Butylbenzylphthalate 31.52 149 4911779 35.45 ug/1 92 41) Benzo(a)anthracene 32.99 228 6878692 37.57 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.30 149 6264424 33.46 ug/1 99 43) Chrysene 33.12 228 6657072 37.07 ug/1 98 45) Di-n-Octylphthalate 35.05 149 9882048 36.71 ug/1 # 96 46) Benzo(b)fluoranthene 36.07 252 5995090 39.33 ug/1 98 47) Benzo(k)fluoranthene 36.14 252 5747849 36.74 ug/1 98 48) Benzo(a)pyrene 36.97 252 5084451 38.37 ug/1 98 49) Indeno(1,2,3-cd)pyrene 40.84 276 5152212 38.88 ug/1 99 5 0) Dibenz(a,h)anthracene 40.90 278 4075014 39.27 ug/1 97 51) Benzo(g,h,i)perylene 41.95 276 4156522 36.71 ug/1 94
(#) = qualifier out of range (m) = manual integration CAL40A.D GCMS1126.M Thu Dec 27 09:53:46 2001 Page 2
NYC-WTC_000019042
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