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GCMS reference material results, Dec 2001

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Laboratory report documenting gas chromatography-mass spectrometry reference material analysis conducted on December 31, 2001.

NYC-WTC_000017894–000017897

Folder label: “GCMS X 12/14/01 A 12/31/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC3101\CAL4 0.D Vial: 2 Acq On 31 Dec 2001 11:56 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 31 16:03 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title •: 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.62 168 1856051 39.27 ug/1 # 83 31) 4-Bromophenyl-phenylether 23.67 248 1014831 38.75 ug/1 # 91 32) Hexachlorobenzene 24.10 284 1149408 39.91 ug/1 98 3 3) Phenanthrene 25.06 178 5477420 38.85 ug/1 99 34) Anthracene 25.20 178 5290937 37.65 ug/1 99 35) Di-n-butylphthalate 27.00 149 7552966 40.26 ug/1 # 99 36) Fluoranthene 28.68 202 5451635 40.06 ug/1 98 39) Pyrene 29.35 202 5601488 37.56 ug/1 98 40) Butylbenzylphthalate 31.51 149 2919487 37.49 ug/1 # 82 41) Benzo(a)anthracene 32.99 228 3935440 38.23 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.30 149 3682695 34.99 ug/1 97 43) Chrysene 33.11 228 3882734 38.46 ug/1 99 45) Di-n-Octylphthalate 35.04 149 5515840 38.51 ug/1 # 91 46) Benzo(b)fluoranthene 36.07 252 3292502 40.60 ug/1 99 47) Benzo(k)fluoranthene 36.14 252 3333463m 40.05 ug/1 4 8) Benzo(a)pyrene 36.96 252 2713907 38.49 ug/1 97 49) Indeno(l,2,3-cd)pyrene 40.84 276 2575936 36.54 ug/1 96 5 0) Dibenz(a,h)anthracene 40.89 278 2032353 36.81 ug/1 96 51) Benzo(g,h,i)perylene 41.94 276 2064920 34.28 ug/1 92

(#) = qualifier out of range (m) = manual integration CAL40.D GCMS1126.M Mon Dec 31 16:04:18 2001 Page 2

NYC-WTC_0000 17896

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NYC-WTC_000017896Source: NYC Law Department, mirrored locally

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