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GCMS calibration data sheet, Dec 2001

Machine-extracted title · confidence 95%

Document showing calibration results for GCMS analysis of volatile organic compounds on December 27, 2001.

NYC-WTC_000017654–000017657

Folder label: “GCMS X 12/13/01 A 12/27/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC2 701\CALI0 0.D Vial: 2 Acq On 27 Dec 2001 9:30 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 28 14:27 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update ’: Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.65 168 3017767 100.21 ug/1 # 84 31) 4-Bromophenyl-phenylether 23.69 248 1645497 98.62 ug/1 95 32) Hexachlorobenzene 24.11 284 1837286 100.13 ug/1 92 3 3) Phenanthrene 25.08 178 8790445 97.85 ug/1 98 3 4) Anthracene 25.22 178 8918772 99.60 ug/1 99 35) Di-n-butylphthalate 27.02 149 12119597 101.39 ug/1 # 99 3 6) Fluoranthene 28.70 202 9154721 105.57 ug/1 97 39) Pyrene 29.37 202 9314038 89.56 ug/1 99 40) Butylbenzylphthalate 31.53 149 5083659 93.59 ug/1 87 41) Benzo(a)anthracene 33.00 228 7060067 98.34 ug/1 98 42) Bis(2-ethylhexyl)phthalate 33.32 149 6493183 88.47 ug/1 98 43) Chrysene 33.14 228 6886356 97.81 ug/1 98 45) Di-n-Octylphthalate 35.06 149 10526727 92.47 ug/1 # 93 46) Benzo(b)fluoranthene 36.09 252 6357828 98.65 ug/1 99 4 7) Benzo(k)fluoranthene 36.16 252 5945548m 89.88 ug/1 48) Benzo(a)pyrene 36.99 252 5823945 103.94 ug'/l 99 49) Indeno(l,2,3-cd)pyrene 40.88 276 5939427 106.00 ug/1 98 50) Dibenz(a,h)anthracene 40.95 278 4632713 105.58 ug/1 97 51) Benzo(g,h,i)perylene 42.00 276 4831466 100.91 ug/1 93

(#) = qualifier out of range (m) = manual integration CAL100.D GCMS1126.M Fri Dec 28 14:27:59 2001 Page 2

NYC-WTC_000017656

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NYC-WTC_000017656Source: NYC Law Department, mirrored locally

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