GCMS calibration data sheet, Dec 2001

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC2 701\CAL10 0.D Vial: 2 Acq On 27 Dec 2001 9:30 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 28 14:27 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.69 152 620379 20.00 ug/1 -0.01 10) Naphthalene-d8 15.30 136 2400846 20.00 ug/1 -0.01 17) Acenaphthene-diO 20.57 164 1143049 20.00 ug/1 -0.01 29) Phenanthrene-diO 25.00 188 1696288 20.00 ug/1 0.00 38) Chrysene-dl2 33.04 240 1204908 20.00 ug/1 0.00 44) Perylene-dl2 37.13 264 856730 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 29.90 235 14888 0.61 ug/mL -0.17 Spiked Amount 5.000 Recovery = 12.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.43 74 3302035 121.02 ug/1 78 3) bis(2-Chloroethyl)ether 11.13 93 4705944 109.89 ug/1 92 4) 1,3-Dichlorobenzene 11.59 146 4502357 99.79 ug/1 98 5) 1,4-Dichlorobenzene 11.73 146 4514926 98.96 ug'/l 99 6) 1,2-Dichlorobenzene 12.24 146 4155237 98.76 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 12.59 45 6943729 127.33 ug/1 96 8) N-Nitroso-di-n-propylamine 13.01 70 3089283 126.63 ug/1 92 9) Hexachloroethane 13.07 117 1885619 113.63 ug/1 93 11) Nitrobenzene 13.39 77 4722579 (126.20 ug/1 89 12) 1sophorone 14.05 82 8562022 118.76 ug/1 94 13) bis(2-Chloroethoxy)methane 14.73 93 5363039 110.73 ug/1 99 14) 1,2,4-Trichlorobenzene 15.19 180 3363937 96.49 ug/1 99 15) Naphthalene 15.36 128 11183592 97.48 ug/1 100 16) Hexachlorobutadiene 15.89 225 1705232 100.37 ug/1 100 18) Hexachlorocyclopentadiene 18.08 237 927138 112.59 ug/1 98 19) 2-Chloronaphthalene 18.85 162 6324548 96.99 ug/1 95 20) Dimethylphthalate 19.98 163 7584294 99.84 ug/1 100 21) 2,6-Dinitrotoluene 20.20 165 1852781 103.22 ug/1 # 62 22) Acenaphthylene 20.12 152 9046671 98.72 ug/1 100 2 3) Acenaphthene 20.68 153 6322327 96.48 ug/1 99 24) 2,4-Dinitrotoluene 21.36 165 2418957 106.00 ug/1 # 76 25) Diethylphthalate 22.12 149 7330129 104.28 ug/1 98 26) 4-Chlorophenyl-phenylether 22.23 204 2816363 91.78 ug/1 92 2 7) Fluorene 22.20 166 6100354 90.72 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 22.70 77 9109525 42 ug/L # 90

(#) = qualifier out of range (m) = manual integration CAL100.D GCMS1126.M Fri Dec 28 14:27:55 2001 Page 1

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