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GCMS calibration verification results, Dec 2001

Machine-extracted title · confidence 95%

Laboratory report of GCMS calibration verification for sample AD29665 conducted on December 15, 2001.

NYC-WTC_000036963–000036966

Folder label: “GCMS X 12/10/01 A 12/15/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC14 01\CAL25A.D Vial: 2 Acq On 15 Dec 2001 3:30 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 2 9:30 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.61 168 1360864 25.04 ug/1 # 92 31) 4-Bromophenyl-phenylether 23.66 248 768421 25.52 ug/1 98 32) Hexachlorobenzene 24.08 284 884556 26.71 ug/1 98 3 3) Phenanthrene 25.05 178 4048554 24.97 ug/1 99 34) Anthracene 25.19 178 3955610 24.48 ug/1 99 35) Di-n-butylphthalate 26.99 149 5526120 25.61 ug/1 100 36) Fluoranthene 28.67 202 4009466 25.62 ug/1 99 3 9) Pyrene 29.33 202 4114238 23.29 ug/1 99 40) Butylbenzylphthalate 31.50 149 2117218 22.95 ug/1 93 41) Benzo(a)anthracene 32.97 228 2983711 24.47 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.29 149 2739573 21.98 ug/1 99 43) Chrysene 33.10 228 2916166 24.39 ug/1 99 45) Di-n-Octylphthalate 35.04 149 4010330 21.67 ug/1 # 95 46) Benzo(b)fluoranthene 36.05 252 2656927 25.36 ug/1 99 47) Benzo(k)fluoranthene 36.11 252 2825695 26.28 ug/1 100 48) Benzo(a)pyrene 36.94 252 2221003 24.38 ug/1 99 49) Indeno(l,2,3-cd)pyrene 40.79 276 2077048 22.80 ug/1 96 50) Dibenz(a,h)anthracene 40.86 278 1645838 23.08 ug/1 96 51) Benzo(g,h,i)perylene 41.89 276 1697147 21.81 ug/1 93

(#) = qualifier out of range (m) = manual integration CAL25A.D GCMS1126.M Wed Jan 02 09:31:00 2002 Page 2

NYC-WTC_000036965

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NYC-WTC_000036965Source: NYC Law Department, mirrored locally

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