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GCMS reference standard results, Jan 2002

Machine-extracted title · confidence 88%

Reference standard analysis report verifying instrument performance for volatile organic compound testing in early 2002.

NYC-WTC_000016694–000016698

Folder label: “GCMS X 12/12/01 A 12/19/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC1901\REF.D Vial: 4 Acq On : 19 Dec 2001 12:41 pm Operator: 209 GALOS Sample : gc/ms scan 12/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 19 13:29 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.59 168 119097 2.82 ug/1 # 86 31) 4-Bromophenyl-phenylether 23.66 248 83502 3.57 ug/1 95 32) Hexachlorobenzene 24.07 284 95310 3.70 ug/1 98 3 3) Phenanthrene 25.04 178 473111 3.75 ug/1 99 34) Anthracene 25.17 178 423584 3.37 ug/1 99 35) Di-n-butylphthalate 26.99 149 695669 4.15 ug/1 # 99 36) Fluoranthene 28.65 202 436714 3.59 ug/1 96 39) Pyrene 29.32 202 458910 3.42 ug/1 99 40) Butylbenzylphthalate 31.50 149 212123 3.03 ug/1 92 41) Benzo(a)anthracene 32.96 228 321029 3.47 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.29 149 643468 6.80 ug/1 99 43) Chrysene 33.09 228 364885 4.02 ug/1 100 45) Di-n-Octylphthalate 35.03 149 321286 2.37 ug/1 # 90 4 6) Benzo(b)fluoranthene 36.04 252 283788 3.70 ug/1 98 47) Benzo(k)fluoranthene 36.10 252 327036 4.15 ug/1 99 4 8) Benzo(a)pyrene 36.93 252 196369 2.94 ug/1 97 49) Indeno (1,2,3-cd) pyrene 40.80 276 190782 2.86 ug/1 96 50) Dibenz(a,h)anthracene 40.85 278 161010 3.08 ug/1 97 51) Benzo (g,h,i)perylene 41.88 276 167512 2.94 ug/1 95

(#) = qualifier out of range (m) = manual integration REF.D GCMS1126.M Thu Jan 03 10:05:08 2002 Page 2

NYC-WTC_0000 16697

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NYC-WTC_000016697Source: NYC Law Department, mirrored locally

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