GCMS calibration results for sample AD31586, January 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\JAN03 02\CAL10 0.D Vial: 7 Acq On 3 Jan 2002 4:25 pm Operator: 209 GALOS Sample mix Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Feb 1 9:37 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.55 152 983899 20.00 ug/1 -0.15 10) Naphthalene-d8 15.15 136 3922872 20.00 ug/1 -0.15 17) Acenaphthene-dlO 20.40 164 1985153 20.00 ug/1 -0.17 29) Phenanthrene-diO 24.84 188 2932822 20.00 ug/1 -0.15 38) Chrysene-dl2 32.87 240 1613391 20.00 ug/1 -0.16 44) Perylene-dl2 36.93 264 877141 20.00 ug/1 -0.19

System Monitoring Compounds 37) 2,4-DDD 0.00 235 Od 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.34 74 4869846m 112.54 ug/1 3) bis(2-Chloroethyl)ether 11.01 93 7699017 113.36 ug/1 96 4) 1,3-Dichlorobenzene 11.44 146 6563478 91.73 ug/1 100 5) 1,4-Dichlorobenzene 11.59 146 6471419 89.43 ug/1 99 6) 1,2-Dichlorobenzene 12.11. 146 5780231 86.62 ug/1 99 7) 2,2’-oxybi s(1-Chloropropan 12.45 45 10124616 117.06 ug/1 98 8) N-Nitroso-di-n-propylamine 12.90 70 4320668 111.67 ug/1 97 9) Hexachloroethane 12.92 117 2568457 97.59 ug/1 98 11) Nitrobenzene 13.25 77 7352045 120.24 ug/1 97 12) 1sophorone 13.93 82 13764780 116.85 ug/1 99 13) bis(2-Chloroethoxy)methane 14.59 93 8537954 107.89 ug/1 100 14) 1,2,4-Trichlorobenzene 15.04 180 5048032 88.62 ug/1 99 15) Naphthalene 15.23 128 15987449 85.29 ug/1 99 16) Hexachiorobutadiene 15.75 225 ______ 2464783 __ _ ug/1 98 18) Hexachlorocyclopentadiene 17.92 237 1932948 135.15 ug/1 98 19) 2-Chioronaphthalene 18.71 162 9534744m 84.19 ug/1 20) Dimethylphthalate 19.85 163 11929396 90.42 ug/1 100 21) 2,6-Dinitrotoluene 20.07 165 2995310 96.09 ug/1 94 22) Acenaphthylene 19.96 152 14393250 90.43 ug/1 100 2 3) Acenaphthene 20.53 153 9349991 82.16 ug/1 100 24) 2,4-Dinitrotoluene 21.24 165 3993321 100.76 ug/1 92 25) Diethylphthalate 21.99 149 11078169m 90.75 ug/1 26) 4-Chlorophenyl-phenylether 22.08 204 4012308 75.29 ug/1 98 27) Fluorene 22.05 166 8763643 $75.04 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 22.56 77 13782445 109.26 ug/L 99

(#) = qualifier out of range (m) = manual integration CAL100.D GCMS1126.M Fri Feb 01 09:37:58 2002 Page 1

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