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GCMS calibration results for sample AD31586, January 2002

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Laboratory report of GCMS calibration data for sample AD31586 listing chemical standards and response values.

NYC-WTC_000049675–000049678

Folder label: “GCMS X 1/2/02 A 1/3 - 1/4/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\JAN03 02\CAL10 0.D Vial: 7 Acq On 3 Jan 2002 4:25 pm Operator: 209 GALOS Sample mix Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Feb 1 9:37 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.52 168 4408606 84.67 ug/1 # 85 31) 4-Bromophenyl-phenylether 23.53 248 2522854 87.45 ug/1 99 32) Hexachlorobenzene 23.96 284 2776715 87.52 ug/1 99 3 3) Phenanthrene 24.93 178 13485817 86.82 ug/1 100 34) Anthracene 25.07 178 13717845 88.60 ug/1 100 35) Di-n-butylphthalate 26.87 149 17751769 85.89 ug/1 98 36) Fluoranthene 28.54 202 13738497 91.63 ug/1 100 3 9) Pyrene 29.21 202 13880056 99.67 ug/1 99 40) Butylbenzylphthalate 31.38 149 7425844 102.10 ug/1 97 41) Benzo(a)anthracene 32.84 228 9110407 94.77 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.16 149 8599940 87.50 ug/1 99 43) Chrysene 32.97 228 8949651 94.93 ug/1 99 45) Di-n-Octylphthalate 34.91 149 12941873 111.04 ug/1 98 46) Benzo(b)fluoranthene 35.92 252 7835109 118.74 ug/1 99 47) Benzo(k)fluoranthene 35.99 252 6976650m 103.01 Ug/1 4 8) Benzo(a)pyrene 36.79 252 6179282 107.71 ug/1 99 4 9) Indeno(1,2,3-cd)pyrene 40.55 276 5673449 98.89 ug/1 99 5 0) Dibenz(a,h)anthracene 40.61 278 4358540 97.02 ug/1 99 51) Benzo(g,h,i)perylene 41.64 276 4534989 92.52 ug/1 99

(#) = qualifier out of range (m) = manual integration CAL100.D GCMS1126.M Fri Feb 01 09:38:01 2002 Page 2

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