GC/MS calibration results, PAH compounds, May 2002

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GC/MS instrument calibration report for polycyclic aromatic hydrocarbons and chlorinated compounds using 40 µg/L standards, dated May 2-3, 2002.

NYC-WTC_000045526–000045542

Folder label: “GCMS X 5/3/02 A 5/8/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAY0 2 02\9451.D Vial: 10 Acq On 2 May 2002 11:38 pm Operator: Sample GC/MS SCAN 4/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 8 2-Hexanone, 3-hydroxy-3,5-dime Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 9.14 59.50 ug/1 5371760 1,4-Dichlorobenzene-d4 12.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone, 3-hydroxy-3,5-dimethyl- 144 C8H1602 006321-14-8 39 2 Amylene/Hydrate 88 C5H120 000075-85-4 38 3 2-Pentanol, 2-methyl- 102 C6H140 000590-36-3 38 4 2-Propanol, 2-methyl-________________ 74 C4H10O 000075-65-0 36 Abundance Scan 447 (9.139 min): 9451.D (-) m/z 59.05 100.00% 59

5000 43 ' 1 I ' ' ' ' 1 1 ' 1 ' I ' r 1 1 i ' 1 1 1 1 1

, 69 80 87 95 107 121 136 151 8.80 9.00 9.20 9.40 ,,,,,,, , 364, , 51 1 r1'1 I I 1 I I I I 1 I 1 I I 1 1 CT-B-mpn/n/nd/ I I I I I I I [ I I t I l I I I I I ■ I I I I I m/z 43.05 37.27% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #8436: 2-Hexanone, 3-hydroxy-3,5-dimethyl- 59

5000 / 1 1 i 1 1 1 1 i 1 1 ' ' i 1 • r 1 i 1 1 1 1 i 1 8.80 9.00 9.20 9.40 43 m/z 41.05 16.57% 101

m/z-> 20 -i । i i i ' । । i o 1, i । । r

30 40 50 1H 60 69 70 83 I m 1 I [ ii ii । । > i । I । । । । । i । । । । । । 1 । । i i i । i ii i [ i i i i । i r 80 90 100 110 120 130 140 150 160 Abundance #62938: Amylene Hydrate 53 ...................... ) . । । ] । । । । [ i । । । | । i i । | i i i i I | i

8.80 9.00 9.20 9.40 73 5000 m/z 150.95 6.06% 31 43 A m/z-> ‘tdt 20 30 40 + I [ । r I I | i I I । ।11 I I I | 1 I I I [ I i t I | i I “I"r' | i I n 1

50 60 70 80 90 100 110 120 130 140 150 160 Abundance #63532: 2-Pentanol, 2-methyl- ................... /................ 1 1 1 1 ' ' 1 1 1 ' 1 ' 1 1 / 1 I ' 1 1 ‘ r1 59 8.80 9.00 9.20 9.40 m/z 153.00 5.81%

5000 45 87 31 ... .......... ......................................................................................... . I 1 I ‘ ' 1 : 1 1 ........ /............ I-1 l ) I I I I 111 I I I I I I I I I I I I m/z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 8.80 9.00 9.20 9.40

9451.D GCMS0501.M Fri May 03 08:42:20 2002 Page 8

NYC-WTC_000045538

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