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GC/MS analysis results for sample AD22655, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22655 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087326–000087348

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087335
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22655.D Vial: 14 Acq On : 29 Sep 2001 1:11 am Operator: 209 GALOS Sample : gc/ms unknown Inst GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L

Peak Number 3 3-Hexanol Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

6.63 0.41 ug/1 51468 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexano^ 102 C6H14O 000623-37-0 78 2 Amylene^Hydrate 88 C5H12O 000075-85-4 40 3 Octant, 7-hydroxy-3,7-dimethyl- 172 C10H20O2 000107-75-5 36 4 3-Mntanol 88 C5H12O 000584-02-1 33 Abundance Scan 173 (6.630 min); 22655.D (-) m/ z ioo7do% i 55 5(9

73 5000 43 39 84 6.20 6.40 6.60 6.80 7.00 100 69 , ti+t 44+ I....... -rrtpllilii " I " '' I'' I" " I' ’" I " I' ‘ m/z 55.00 78.71% m/z~> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Sundance #63530; 3-Hexanol 5l9 55 73 5000 I ■ I I I I I I, I I I I I I I I I I I Yf

6,20_j6;4p__6jg__6,80_j:,^^ 31 27 m/z 73.00 53.96% 45 pT-T-rp-irry-r-rry 84 +h +4 1‘ 1 r”’I"'•I in/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #849: Amylene Hydrate 59 , , .ii???qA1 ■ I I I I I 55 6.20 6.40 6.60 6.80 7.00 5000 73 m/z 4 2.95 27.91% 31 27 45 '37 I ! m/z-> Abundance 20 I'''' I '' " I I‘ 'I I"’J'"'I‘ 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 #68361: Octanal, 7-hydroxy-3,7-dimettiyl- 'I AJ _6;20__640__6,6p__6J0__Y0^ 43 m/z 41.05 25.92% 5000 71

I II 67 I 96 H ' I " " I " " I " " I' I I ’ I ' " ■ I " " I * I I I I " " I " ' I 11 " ' I ' " 11 I ' " I " ' I I " " I I I I 111 I I 11 I I rn/z-> 2°---25._30_ 35 40 45 50 65 70 75 80 85 90 95 100 105 6.20 ' 6.40' ' 6.60 6.80 7.00 |

22655.D NP091101.M Wed Oct 10 14:46:02 2001 Page 3

NYC-WTC_000087335

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