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GC/MS analysis results for sample AD22655, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22655 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087326–000087348

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087336
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22655.D Vial: 14 Acq On : 29 Sep 2001 1:11 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

6.74 0.50 ug/1 62294 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hex^ol 102 C6H14O 000626-93-7 83 2 2-Pehranol, 4-methyl- 102 C6H14O 000108-11-2 74 3 2-H=xanol, (R)- 102 C6H14O 026549-24-6 43 4 ^^Hexanol /_ _ _(S) - _________________ _ 102 C6H14O _____ 052019-78-0 43 'Abuiwance ' Scan 185 (6?74b mln): 22655,0 (-) m/z 45”05 100.00% 4)5

5000 ... ................ 41 69 56 6.40 6,60 6,80 7,00 ....... .. ....... 11' •" I b I' I' I 84 87 ' I''' I ('' I' I'''' I''' 11'''' I'''' I' m/z 69.00 17.26% -n/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1792: 2-Hexanol 4^

5000 -■'■'■I '

6.40 6,60 6.80 7,00 41.00 14.49% 55 58 69 84 87 T" " I.. m/z-> 10 15 20 25 30 35 40 45 50 55 60 6,5 70 75 80 8.5 90 9,5 •Abundance - #63545: 2-Pentano!. 4-methyl- 45

6.40 6.60 6,80 7,00 5000 m/z 42.95 10.61% 69 ’»~27 3942 57 ! 84 87 ' I'''' I''' • I'' " I'''' I'''' I'''' I " '' I'''' I' " ' I''' • I' ‘' m/2-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1794: 2-Hexanol, (R)- 43 6,40 6,60 6.80 7,00 m/z 43.90 10.55% 5000

69 ...... }?,........Lip....... .................. 55 ..... Il.n,, 84 87 '' I' ‘' I'' I I I I I I I I I I > I I I I << I I . I I

m/2~> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6,40 6,60 6,80 7,00

22655.D NP091101.M Wed Oct 10 14:46:07 2001 Page 4

NYC-WTC_000087‘336

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NYC-WTC_000087336Source: NYC Law Department, mirrored locally

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