GC/MS calibration results, PAH compounds, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAY0202\9451.D Vial: 10 Acq On 2 May 2002 11:38 pm Operator: Sample GC/MS SCAN 4/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************** Peak Number 7 2-Propanone, 1,1,1-trichloro- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

8.23 1.50 ug/1 135408 1,4-Dichlorobenzene-d4 12.20

Hit# of 5 / Tentative ID MW MolForm CAS# Qual

1 2 - Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 37 2 2-Propanone, 1,1-dichloro- 126 C3H4C120 000513-88-2 9 3 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 4 4 1-Eicosanol 298 C2OH420 000629-96-9 4 Abundance Scan 348 (8.232 min): 9451 .D (-) m/z 43.05 100.00% 43

5000

7.80 8.00 8.20 8.40 8.60 37 , ,49 63_____ 83 .. ......................................................... 97 Ill................... 1,1, 117 125 ......................... 1 m/z 124.95 8.51% ■ 1 i 1 ■ 1 1 i 1 ' 1 1 i ' -TT tii।iiiili। । । ini।tIiipiii।IJi। । ।ri। । ।ni।ir m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000 7.80 8.00 8.20 8.40 8.60 m/z 97.00 6.47% 15 35 49 85 97 117 125 I [ i i i i i -i i i "i i i < i ~ i I i i । I I । i'। i i i i | I I । ’ i ’ । i ill | TT ■ 1 I ' ' 1 ■।111■ i ■ ''' । ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #64841: 2-Propanone, 1,1-dichloro- 43 I 1 I I I I I I I I I ■ I I ■ I 1 I I I I I I I

7.80 8.00 8.20 8.40 8.60 5000 m/z 46.95 5.73%

27 . ___________ । 30 49 1 i ■ ■ ■ ■ । 63■ ■ ■ । ■ ■ ■ ■ । 83 ■ ■ 91 ■' 126 i■ ■ ■ ■ ■ । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ ■' ■' 11111 111111' ।111111 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4732: N-Acetylpyrrolidone WA AAA A AM A/“W AA I III I I II I I I I I I I I I ! II 101007 43 7.80 8.00 8.20 8.40 8.60 m/z 82.95 5.22%

5000 99 127 56 86 _ 30 | ----- H 6f.... Il..... l 112 1 i ■ • 1 1 i 1 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 7.80 8.00 8.20 8.40 8.60

9451.D GCMS0501.M Fri May 03 08:42:19 2002 Page 7

NYC-WTC_000045537