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GCMS calibration results for deuterated standards, May 2 2002

Machine-extracted title · confidence 100%

Calibration scan report for EPA Method 508 showing retention times and deviations for deuterated standards on May 2 2002.

NYC-WTC_000044458–000044460

Folder label: “GCMS X 4/29/02 A 5/1/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\1\DATA\050102\CAL10.D Vial: 3 Acq On 1 May 2002 11:20 am Operator: Mclean Sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 02 09:45:22 2002 Quant Results File: 050102.RES Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Thu May 02 09:38:23 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue 36) Fluoroanthene 26.54 202 5042928 11.69 ug/L 98 38) Pyrene 27.17 202 4889774 10.96 ug/L 98 39) Butylbenzylphthalate 29.53 149 1587559 7.99 ug/L 96 40) Benzo(a)anthracene 30.79 228 3637589 10.24 ug/L 98 41) Bis(2-ethylhexyl)phthalate 31.40 149 1982375 7.38 ug/L 96 42) Chrysene 30.88 228 4075004m 11.11 ug/L 44) Di-n-octylphthalate 33.24 149 2078727m 6.80 ug/L 45) Benzo(b)fluoranthene 33.75 252 3076913 10.70 ug/L 96 46) Benzo(k)fluoranthene 33.83 252 4330786 11.94 ug/L 97 47) Benzo(a)pyrene 34.55 252 2914061 10.29 ug/L 98 48) Indeno(1,2,3-cd)pyrene 37.39 276 1434128 7.13 ug/L 95 49) Dibenz(a,h)anthracene 37.51 278 1843240 8.61 ug/L 97 50) Benzo(g,h,i)perylene 38.13 276 2242412 10.11 ug/L 98

(#) = qualifier out of range (m) = manual integration (+) = signals summed CAL10.D 050102.M Thu May 02 09:46:28 2002 Page 2

NYC-WTC_000044459

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NYC-WTC_000044459Source: NYC Law Department, mirrored locally

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