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GCMS calibration results for deuterated standards, May 2 2002

Machine-extracted title · confidence 100%

Calibration scan report for EPA Method 508 showing retention times and deviations for deuterated standards on May 2 2002.

NYC-WTC_000044461–000044463

Folder label: “GCMS X 4/29/02 A 5/1/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\1\DATA\050102\CAL5 0 . D Vial: 5 Acq On 1 May 2002 12:57 pm Operator: Mclean Sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 02 09:41:47 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Thu May 02 09:38:23 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoroanthene 26.56 202 24673855 50.26 ug/L 100 38) Pyrene 27.19 202 23923040 51.40 ug/L 99 39) Butylbenzylphthalate 29.54 149 11649974 56.21 ug/L 98 40) Benzo(a)anthracene 30.80 228 19842020 53.56 ug/L 99 41) Bis(2-ethylhexyl)phthalate 31.40 149 15793960 56.38 ug/L 96 42) Chrysene 30.91 228 19356631m 50.56 ug/L 44) Di-n-octylphthalate 33.26 149 21848538m 58.42 ug/L 45) Benzo(b)fluoranthene 33 . 78 252 17199752 57.27 ug/L 96 46) Benzo(k)fluoranthene 33.86 252 18845857 49.77 ug/L 97 47) Benzo(a)pyrene 34.58 252 16488499 55.75 ug/L 97 48) Indeno(1,2,3-cd)pyrene 37.42 276 11103420 52.86 ug/L 98 49) Dibenz(a,h)anthracene 37.54 278 11586240 51.86 ug/L 100 50) Benzo(g,h,i)perylene 38.18 276 12092244 52.24 ug/L 100

(#) = qualifier out of range (m) = manual integration (+) = signals summed CAL50.D 050102.M Thu May 02 09:42:37 2002 Page 2

NYC-WTC_000044462

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NYC-WTC_000044462Source: NYC Law Department, mirrored locally

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