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GCMS calibration verification results, sample AE11410, May 22 2002

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Laboratory report documenting GCMS calibration verification for sample AE11410 conducted on May 22, 2002.

NYC-WTC_000025234–000025237

Folder label: “GCMS X 5/15/02 A 5/18/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\1\DATA\0 517 02\CALS 0.D Vial: 2 Acq On 17 May 2002 10:34 am Operator: Mclean Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 22 09:38:27 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title .: 508 Modified GC/MS scan Last Update : Wed May 22 09:38:22 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoroanthene 26.54 202 19769811 50.20 ug/L 99 3 8) Pyrene 27.18 202 19145979 51.61 ug/L 98 39) Butylbenzylphthalate 29.53 149 8012499 48.47 ug/L 98 40) Benzo(a)anthracene 30.79 228 15037169 50.91 ug/L 98 41) Bis(2-ethylhexyl)phthalate 31.39 149 10511266 47.05 ug/L 97 42) Chrysene 30.89 228 15782458m 51.61 ug/L 44) Di-n-octylphthalate 33.24 149 14501664 54.84 ug/L 98 45) Benzo(b)fluoranthene 33.76 252 12464189m 57.46 ug/L 46) Benzo(k)fluoranthene 33.83 252 14889860 54.63 ug/L 98 47) Benzo(a)pyrene 34.56 252 11183014 51.66 ug/L 99 48) Indeno(1,2,3-cd)pyrene 37.40 276 7834562 51.62 ug/L 99 49) Dibenz(a,h)anthracene 37.52 278 8708007 53.94 ug/L 99 50) Benzo(g,h,i)perylene 38.15 276 9540299 56.29 ug/L 98

(#) = qualifier out of range (m) = manual integration (+) = signals summed CAL50.D 050102.M Wed May 22 09:39:00 2002 Page 2

NYC-WTC_000025236

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NYC-WTC_000025236Source: NYC Law Department, mirrored locally

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