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GCMS calibration results for deuterated standards, May 2 2002

Machine-extracted title · confidence 100%

Calibration scan report for EPA Method 508 showing retention times and deviations for deuterated standards on May 2 2002.

NYC-WTC_000044464–000044466

Folder label: “GCMS X 4/29/02 A 5/1/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\050102\CAL80 .D Vial: 6 Acq On 1 May 2002 1:46 pm Operator: Mclean Sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 02 09:40:47 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Thu May 02 09:38:23 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoroanthene 26.57 202 30878144 71.49 ug/L 99 3 8) Pyrene 27.20 202 29750374 77.02 ug/L 100 39) Butylbenzylphthalate 29.55 149 15023796 87.33 ug/L 97 40) Benzo(a)anthracene 30.81 228 24897958 80.97 ug/L 98 41) Bis(2-ethylhexyl)phthalate 31.41 149 20638872 88.76 ug/L 95 42) Chrysene 30.92 228 24081101m 75.79 ug/L 44) Di-n-octylphthalate 33.27 149 34746346 100.21 ug/L 98 45) Benzo(b)fluoranthene 33.78 252 22695498 81.50 ug/L 96 46) Benzo(k)fluoranthene 33.87 252 24454605 69.65 ug/L 96 47) Benzo(a)pyrene 34.59 252 22121870 80.67 ug/L 97 48) Indeno(1,2,3-cd)pyrene 37.44 276 17033862 87.46 ug/L 100 .49) Dibenz (a, h) anthracene 37.56 278 17372347 83.87 ug/L 98 50) Benzo(g,h,i)perylene 38.20 276 18147349 84.56 ug/L 100

(#) = qualifier out of range (m) = manual integration (+) = signals summed CAL80.D 050102.M Thu May 02 09:41:39 2002 Page 2

NYC-WTC_000044465

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NYC-WTC_000044465Source: NYC Law Department, mirrored locally

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