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GCMS calibration results for deuterated standards, May 2 2002

Machine-extracted title · confidence 100%

Calibration data for GCMS analysis of volatile organic compounds with response factors recorded on May 2 2002.

NYC-WTC_000044455–000044457

Folder label: “GCMS X 4/29/02 A 5/1/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\050102\CAL5.D Vial: 2 Acq On 1 May 2002 10:30 am Operator: Mclean Sample Inst' Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 02 09:43:37 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Thu May 02 09:38:23 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoroanthene 26.54 202 1841545 5.39 ug/L 99 38) Pyrene 27.17 202 1784533 5.24 ug/L 99 39) Butylbenzylphthalate 29.53 149 369781 <2.44uq / L 97 40) Benzo(a)anthracene 30.79 228 1248746 4.60 ug/L 98 41) Bis(2-ethylhexyl)phthalate 31.39 149 425437 <2.07 g/L 96 42) Chrysene 30.88 228 1519404m 5.42ug/L 44) Di-n-octylphthalate 33.23 149 370570m 1.48 uq/L 45) Benzo(b)fluoranthene 33.75 252 769727 3.82 ug/L 96 46) Benzo(k)fluoranthene 33.82 252 1430846 5.63 ug/L 96 47) Benzo(a)pyrene 34.55 252 849011m 428 ug/L 48) Indeno(1,2,3-cd)pyrene 37.39 276 286560m 2 . 03 ug/L 49) Dibenz(a,h)anthracene 37.50 278 397532m 2.65 ug/L 50) Benzo(g,h,i)perylene 38.13 276 623306m 4.01 ug/L

(#) = qualifier out of range (m) = manual integration (+) = signals summed CAL5.D 050102.M Thu May 02 09:45:12 2002 Page 2

NYC-WTC_000044456

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NYC-WTC_000044456Source: NYC Law Department, mirrored locally

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