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GCMS calibration results for deuterated standards, May 2 2002

Machine-extracted title · confidence 100%

Calibration scan report for EPA Method 508 showing retention times and deviations for deuterated standards on May 2 2002.

NYC-WTC_000044467–000044469

Folder label: “GCMS X 4/29/02 A 5/1/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\1\DATA\05 0102\CAL16 0.D Vial : 7 Acq On 1 May 2002 2:35 pm Operator: Mclean Sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 02 09:39:46 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Thu May 02 09:38:23 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoroanthene 26.59 202 52916683 117.43 ug/L 99 38) Pyrene 27.23 202 51547204 131.76 ug/L 100 39) Butylbenzylphthalate 29.56 149 27631357 158.59 ug/L 97 40) Benzo(a)anthracene 30.84 228 46253300 148.52 ug/L 99 41) Bis(2-ethylhexyl)phthalate 31.42 149 37659890 159.92 ug/L 96 42) Chrysene 30.95 228 42801690m 133.01 ug/L 44) Di-n-octylphthalate 33.28 149 66934085 176.57 ug/L # 95 45) Benzo(b)fluoranthene 33.81 252 42894780 140.90 ug/L 96 46) Benzo(k)fluoranthene 33.91 252 43021893 112.09 ug/L 97 47) Benzo(a)pyrene 34.63 252 41789053 139.39 ug/L 97 48) Indeno(1,2,3-cd)pyrene 37.48 276 35536222 166.90 ug/L 98 49) Dibenz(a,h)anthracene 37.60 278 35445277 156.53 ug/L 99 50) Benzo(g,h,i)perylene 38.26 276 35470269 151.19 ug/L 99

(#) = qualifier out of range (m) = manual integration (+) = signals summed CAL160.D 050102.M Thu May 02 09:40:37 2002 Page 2

NYC-WTC_000044468

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NYC-WTC_000044468Source: NYC Law Department, mirrored locally

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