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GCMS calibration results, June 5 2002

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Calibration verification data for volatile organic compound analysis using gas chromatography-mass spectrometry on June 5, 2002.

NYC-WTC_000015524–000015527

Folder label: “GCMS X 6/4/02 A 6/4/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File C:\MSDCHEM\1\DATA\060402\C4.D Vial: 2 Acq On 4 Jun 2002 4:40 pm Operator: McLean Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Jun 05 14:47:36 2002 Quant Results File: 060302.RES Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Wed Jun 05 14:47:27 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue 36) Fluoroanthene 26.51 202 33158057 88.90 ug/L 99 3 8) Pyrene 27.15 202 31818201 81.41 ug/L 98 39) Butylbenzylphthalate 29.49 149 13702748 83.56 ug/L 99 4 0) Benzo(a)anthracene 30.75 228 24732084 89.76 ug/L 99 41) Bis(2-ethylhexyl)phthalate 31.34 149 17040375 86.49 ug/L 99 42) Chrysene 30.85 228 24548922m 83.87 ug/L 44) Di-n-octylphthalate 33.20 149 25010733 84.88 ug/L 98 45) Benzo(b)fluoranthene 33.72 252 20372356 89.67 ug/L 99 46) Benzo(k)fluoranthene 33.80 252 22911538 84.00 ug/L 99 47) Benzo(a)pyrene 34.52 252 18542496 85.51 ug/L 99 48) Indeno(1,2,3-cd)pyrene 37.35 276 13752848 93.90 ug/L 99 49) Dibenz(a,h)anthracene 37.47 278 14722535 91.50 ug/L 100 50) Benzo(g,h,i)perylene 38.10 276 15301120 89.05 ug/L 99

(#) = qualifier out of range (m) = manual integration (+) = signals summed C4.D 060302.M Wed Jun 05 14:48:12 2002 Page 2

NYC-WTC_000015526

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NYC-WTC_000015526Source: NYC Law Department, mirrored locally

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