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GCMS reference standard results, June 5 2002

Machine-extracted title · confidence 100%

Reference standard analysis report for volatile organic compounds using gas chromatography-mass spectrometry on June 5, 2002.

NYC-WTC_000015528–000015535

Folder label: “GCMS X 6/4/02 A 6/4/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File C:\MSDCHEM\l\DATA\060402\604REFl .D Vial: 4 Acq On 4 Jun 2002 6:18 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Jun 05 12:09:44 2002 Quant Results File: 060302.RES

Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Wed Jun 05 12:03:00 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoroanthene 26.49 202 7195180 17.88 ug/L 98 3 8) Pyrene 27.13 202 7597307 17.45 ug/L 98 39) Butylbenzylphthalate 29.48 149 2076663 18.18 ug/L 96 40) Benzo(a)anthracene 30.74 228 4936124 16.08 ug/L 99 41) Bis(2-ethylhexyl)phthalate 31.34 149 2268622 18.46 ug/L 98 42) Chrysene 30.82 228 5861500m 17.97 ug/L 44) Di-n-octylphthalate 33.19 149 1922774 7.17 ug/L 99 45) Benzo(b)fluoranthene 33.70 252 3813710 15.91 ug/L 98 46) Benzo(k)fluoranthene 33.77 252 5082655 17.66 ug/L 98 47) Benzo(a)pyrene 34.50 252 2792471 12.21 ug/L 99 48) Indeno(l,2,3-cd)pyrene 37.32 276 1657259 10.73 ug/L 99 49) Dibenz(a,h)anthracene 37.44 278 2414185 14.22 ug/L 97 50) Benzo(g,h,i)perylene 38.06 276 2734880 15.09 ug/L 96

(#) = qualifier out of range (m) = manual integration (+) = signals summed 604REF1.D 060302.M Wed Jun 05 12:10:16 2002 Page 2

NYC-WTC_000015531

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NYC-WTC_000015531Source: NYC Law Department, mirrored locally

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