GCMS reference standard results, June 5 2002

Quantitation Report (QT Reviewed) Data File C:\MSDCHEM\1\DATA\060402\604REF1.D Vial: 4 Acq On 4 Jun 2002 6:18 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Jun 5 12:10 2002 Quant Results File: 060302.RES Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Wed Jun 05 12:03:00 2002 Response via : Initial Calibration Abundance TIC:604REF1.D o 2400000- ?2 I o E 2200000- 1 € 2 2000000 f 2 IJI I 2

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1 1200000- § 2 5 J2 Bl % 1 1£ s ? 1 8 S $ g ! i 1000000 .1 2o 8 “ SB- 241 I « § I& I f I 88/8 88 f2S o81 2 C ,23888 R 5. 5 800000 © C g S 12 1 i 1 11 828243 §3 18 If s 836 =®g § s 600000 1 z3°g o- I s § 1 88 % 2 5 s 1 8 1 I I $ C w m * £ & -2 CD E 400000 I 88 X § m

h I X O o Q 5 CXI 200000 CO co t o Q o o Time-> 0 1 ' i 11dp5Te 1 1 1 4.00 6.00 8.00 10.00 1— 12.00 r 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 1 11 32.00 — 34.00 4 1 riar 1 36.00 U 38.00 TTt LO LO o o o o 1 X o s6 — Q 604REF1.D 060302.M Wed Jun.05 12:10:17 2002 Page 3 oo > > 7 7