GCMS reference standard results, June 5 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\1\DATA\060402\604REF2.D Vial: 5 Acq On 4 Jun 2002 7:07 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Jun 05 12:10:23 2002 Quant Results File: 060302.RES Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Wed Jun 05 12:03:00 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-dichlorobenzene-d4 9.90 152 4348973 40.00 ug/L 0.00 10) Napthalene-d8 13.39 136 17369239 40.00 ug/L 0.00 17) Acenapthalene-dlO 18.52 164 9495983 40.00 ug/L 0.00 2 9) Phenanthranene-dl0 22.91 188 14285785 40.00 ug/L 0.00 37) Chrysene-dl2 30.76 240 9204493 40.00 ug/L 0.00 43) Perylene-dl2 34.65 264 5418619 40.00 ug/L 0.00 System Monitoring Compounds 27) TCMX 20.50 209 1999479 :28.75 ug/L 0.00 Spiked Amount 40.000 Recovery 71.88% Target Compounds Qvalue 2) n-nitros-dimethyl amine 3.89 74 182427 2.23 ug/L 93 3) bis(2-Chloroethyl)ether 9.31 93 2185956 13.70 ug/L 98 4) 1,3-Dichlorobenzene 9.73 146 1952922 12.34 ug/L 98 5) 1,4-Dichlorobenzene 9.94 146 2083286 12.13 ug/L 98 6) 1,2-Dichlorobenzene 10.32 146 2040791 13.45 ug/1 98 7) 2,2'oxybis(1-Chloropropane 10.77 45 3575216m 14.14 ug/L 8) N-nitroso-di-propylamine 11.09 70 1613440 14.40 ug/L 98 9) Hexachloroethane 11.22 117 591049 9.06 ug/L 98 11) Nitrobenzene 11.45 77 2146521 13.16 ug/L 98 12) 1sophorone 12.17 82 4810758 16.37 ug/L 99 13) bis(2-Chloroethoxy) methan 12.90 93 2796715 14.33 ug/L 98 14) 1,2,4-Trichlorobenzene 13.26 180 1714266 13.49 ug/L 99 15) Napthalene 13.45 128 7033023 15.83 ug/L 100 16) Hexachlorobutadiene 13.89 225 601279 10.03 ug/L 99 18) 2-Chloronaphthalene 16.89 162 4035504 17.23 ug/L 99 19) Dimethylphthalate 17.96 163 4825188 16.04 ug/L 99 20) 2,6-Dinitrotoluene 18.07 165 747637 14.82 ug/L 95 21) Acenapthylene 18.08 152 6293165 15.88 ug/L 98 22) Acenapthalene 18.61 153 4177887 16.87 ug/L 99 23) 2,4-Dinitrotoluene 19.23 165 997228 14.33 ug/L 92 24) Diethylphthalate 20.10 149 4804126 18.47 ug/L 99 25) 4-Chlorophenyl-phenylether 20.29 204 2309777 16.22 ug/L 98 26) Fluorene 20.16 166 5048711 17.43 ug/L 100 28) Azobenzene 20.74 77 5266837 15.47 ug/L 100 30) Nnitrosodiphenylamine 20.65 169 3177293 19.39 ug/L 99 31) 4-Bromophenyl-phenylether 21.72 248 1186536 16.83 ug/L 99 32) Hexachlorobenzene 21.75 284 1172212 17.38 ug/L 99 3 3) Phenanthrene 22.97 178 7146117 17.42 ug/L 100 34) Anthracene 23.12 178 6865146 16.32 ug/L 99 35) Di-n-butylphthalate 25.05 149 7129424 14.18 ug/L 100 (#) = qualifier out of range (m) = manual integration 604REF2.D 060302.M Wed Jun 05 12:11:00 2002 Page 1

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